Volatile organic compounds results, Mar 4 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\02mar04\0304C10A.D Vial: 17 Acq On 4 Mar 2002 9:45 pm Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 4 22:24 2002 Quant Results File: HP022702.RES Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 28 16:04:48 2002 Response via : Initial Calibration DataAcq Meth : HP022702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1598034 5.00 ug/L -0.09 24) CHLOROBENZENE-D5 21.73 117 1518433 5.00 ug/L -0.10 52) 1,4-DICHLOROBENZENE-D4 26.92 152 704844 5.00 ug/L -0.09 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 604228 5.85 ug/L -0.09 Spiked Amount 5.000 Recovery = 117.00% 3) 4-BROMOFLUOROBENZENE 24.31 174 530440 4.10 ug/L -0.10 Spiked Amount 5.000 Recovery = 82.00% 25) TOLUENE-D8 18.44 98 1982037 5.41 ug/L -0.09 Spiked Amount 5.000 Recovery = 108.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 491837 10.94 ug/L 99 5) CHLOROMETHANE 5.47 50 403692 8.53 ug/L 94 6) VINYL CHLORIDE 5.57 62 260853 10.10 ug/L 96 7) BROMOMETHANE 6.56 94 271113 9.08 ug/L 93 8) CHLOROETHANE 6.70 64 271768 10.28 ug/L 96 9) TRICHLOROFLUOROMETHANE 7.27 101 507946 8.67 ug/L 97 10) Isopropyl Alcohol 7.85 45 3695 2687.10 ug/L 83 12) ACETONE 8.24 43 88807 10.86 ug/L 96 13) 1,1-DICHLOROETHENE 8.58 61 984718 14.15 ug/L 96 14) METHYLENE CHLORIDE 9.59 49 931079 10.72 ug/L 99 15) METHYL TERT BUTYL ETHER 9.89 73 911080 9.69 ug/L 97 16) TRANS-1,2-DICHLOROETHENE 10.25 61 1018621 10.80 ug/L 98 17) 1,1-DICHLOROETHANE 11.15 63 1182450 10.15 ug/L 99 18) 2-BUTANONE (MEK) 11.97 43 135625 7.75 ug/L 98 19) 2,2-DICHLOROPROPANE 12.36 77 771255 8.98 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.46 96 679760 9.48 ug/L 99 21) CHLOROFORM 12.79 83 1169465 9.56 ug/L 99 22) BROMOCHLOROMETHANE 13.16 49 532967 8.84 ug/L 91 23) 1,2-DICHLOROETHANE 14.51 62 758328 9.81 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.69 97 877832 10.81 ug/L 99 27) 1,1-DICHLOROPROPENE 14.01 75 926188 11.64 ug/L 98 28) CARBON TETRACHLORIDE 14.27 117 733123 10.76 ug/L 97 29) BENZENE 14.61 78 2362546 10.49 ug/L 98 30) TRICHLOROETHENE 15.89 95 685467 10.35 ug/L 97 31) 1,2-DICHLOROPROPANE 16.24 63 641609 9.82 ug/L 98 32) DIBROMOMETHANE 16.91 174 272292 7.94 ug/L 80 33) BROMODICHLOROMETHANE 16.75 83 812824 9.91 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.23 63 209848 10.12 ug/L 100 35) METHYL ISO-BUTYL KETONE 17.32 58 104360 8.96 ug/L 97 36) CIS-1,3-DICHLOROPROPENE 17.84 75 863003 9.68 ug/L 97 37) TOLUENE 18.61 91 2483836 10.04 ug/L 100 3 8) TRANS-1,3-DICHLOROPROPENE 18.88 75 611911 9.59 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.27 97 387208 9.11 ug/L 99 40) TETRACHLOROETHENE 20.06 166 609492 8.58 ug/L 98 41) 1,3-DICHLOROPROPANE 19.80 76 762371 9.78 ug/L 99 42) DIBROMOCHLOROMETHANE 20.48 129 448947 8.80 ug/L 98 43) 1,2-DIBROMOETHANE 20.94 107 389967 9.00 ug/L 98 44) CHLOROBENZENE 21.81 112 1561551 9.21 ug/L 95 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 499142 8.87 ug/L 100 46) 2-HEXANONE 19.16 43 184507 6.22 ug/L 96 47) ETHYLBENZENE 21.86 91 2865878 10.20 ug/L 100 (#) = qualifier out of range (m) = manual integration 0304C10A.D HP022702.M Mon Mar 04 22:24:13 2002 Page 1

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