VOC analysis results, sample AE12737, June 2002

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Data File C:\HPCHEM\1\DATA\02JUNE3\0 6 03R5.D Vial 6 Acq On 3 Jun 2002 12:26 pm Operator 201-wb Sample ref 5 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: Jun 7 12:59 2002 Quant Results File: HP052902.RES Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri May 31 14:34:13 2002 Response via : Initial Calibration DataAcq Meth : HP052902.

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1763835 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.75 117 1636984 5.00 ug/L 0.00 52) 1,4-DICHLOROBENZENE-D4 26.93 152 828792 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 730763 4.58 ug/L -0.02 Spiked Amount 5.000 Recovery = 91.60% 3) 4-BROMOFLUOROBENZENE 24.34 174 646148 4.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.00% 25) TOLUENE-D8 18.45 98 2127439 5.16 ug/L -0.02 Spiked Amount ■ 5.000 Recovery = 103.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.85 85 260587 4.14 ug/L . 100 5) CHLOROMETH-ANE 5.36 50 404699 4.14 ug/L 99 6) VINYL CHLORIDE 5.59 62 279556 5.52 ug/L 98 7) BROMOMETHANE 6.57 94 162230 5.87 ug/L 100 8) CHLOROETHANE 6.72 64 228444 5.04 ug/L 98 9) TRICHLOROFLUOROMETHANE 7.27 101 406936 5.42 ug/L 100 10) Isopropyl Alcohol 7.87 45 38841099 23763.19 ug/L, 91 12) ACETONE 8.24 43 306942m 16.68 ug/L 13) 1,1-DICHLOROETHENE 8.60 61 414978 3.27 ug/L 99 14) METHYLENE CHLORIDE 9.60 49 406131 3:44 ug/L 92 15) METHYL TERT BUTYL ETHER 9.91 73 348532 3.82 ug/L 96 16) TRANS-1,2-DICHLOROETHENE 10.27 61 444308 3.41 ug/L 93 17) 1,1-DICHLOROETHANE 11.15 63 538483 3.69 ug/L 99 18) 2-BUTANONE (MEK) 11.99 43 198579 14.42 ug/L 98 19) 2,2-DICHLOROPROPANE 12.38 77 413661 3.80 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.47 96 337061 4.41 ug/L 90 21) CHLOROFORM 12.81 83 637400 4.25 ug/L 99 22) BROMOCHLOROMETHANE 13.18 49 241923 3.76 ug/L 87 23) 1,2-DICHLOROETHANE 14.53 62 444904 4,25 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.69 97 466191 4.40 ug/L 98 27) 1,1-DICHLOROPROPENE 14.02 75 437666 4.38 ug/L 98 28) CARBON TETRACHLORIDE 14.29 117 392352 4.44 ug/L 97 29) BENZENE 14.63 78 1135453 4.64 ug/L 99 3 0) TRICHLOROETHENE 15.91 95 355156 4.84 ug/L 95 31) 1,2-DICHLOROPROPANE 16.27 63 301153 4.68 ug/L 97 32) DIBROMOMETHANE 16.93 174 151237 5.10 ug/L 94 33) BROMODICHLOROMETHANE 16.78 83 449637 4.'88 ug/L 96 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 76670 4.03 ug/L 94 35) METHYL ISO-BUTYL KETONE 17.34 58 169970 18.65 ug/L 95 36) CIS-1,3-DICHLOROPROPENE 17.87 75 409020 4.84 ug/L 98 37) TOLUENE 18.63 91 1301358 5.09 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.91 75 311272 5.14 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.28 97 198749 5.28 ug/L 99 40) TETRACHLOROETHENE 20.07 166 371498 5.26.ug/L 97 41) 1,3-DICHLOROPROPANE 19.83 76 359220 4.88 ug/L 98 42) DIBROMOCHLOROMETHANE 20.51 129 246257 5.37 ug/L 99 43) 1,2-DIBROMOETHANE 20.97 107 191596 5.13 ug/L 94 44) CHLOROBENZENE 21.84 112 876955 5.42 ug/L 93 45) 1,1,1,2-TETRACHLOROETHANE 21.89 131 301399 5.58 ug/L 96 46) 2-HEXANONE 19.18 43 312353 17.57 ug/L 97 47) ETHYLBENZENE 21.89 91 1629987 5.35 ug/L 99 (#) = qualifier out of range (m) = manual integration 0603R5.D HP052902.M Fri Jun 07 13:01:41 2002 Page 1

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