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VOC analysis results, sample AE11905, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE11905 analyzed on May 22, 2002.

NYC-WTC_000083395–000083562

Folder label: “524 5/22/02 - 5/23/02

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Scanned page image, NYC-WTC_000083401
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAY22\0522Bl.D Vial: 1 Acq On : 22 May 2002 9:10 am Operator: 201-wb Sample : lab blank 1 (voc di) Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: GAS6.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ★ it*******************************************************************

Peale Number 1 Cyclotetrasiloxane, octamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22161 0.21 ug/L 151398 CHLOROBENZENE-D5 21.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 74 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N . 027869-56-3 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 5 4 lH-Indole-3-carboxaldehyde, 2-(1,1- 281 C19H23NO 025584-28-5 5 Abundance Scan 1094 (22.610 min); 0522B1.D (-) m/z 281.25 100.00% 2$1

5000

73 133 22.20 22.40 22.60 22.80 23.00 45 I 191 207 249 265 m/z 282.25 33.42% ' I' '' ' I' I'' '' I'' '' I' '' •n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966; Cyclotetrasiloxane, octamethyl- 2*1

5000 ' ' I'''' I' ''' I'' 22.20 22.40 22.60 22.80 23.00 m/z 283.25 20.13% 133 1631771 I 235^^5 | 73 I ' I'''' I' I ' I ' ' ' ■' I ’ ' ’' I ' *■' ' I ' ' ' ' I ' ‘ ' I • ' • ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643; Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2$1

22.20 22.40 22.60 22.80 23.00 5000 m/z 73.05 12.28%

126 I T T I •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602; 6,7-Benzo-phenothiazine-5,5-dioxide 2i!1 22.20 22.40 22.60 22.80 23.00 m/z 133.15 11.88% . A 5000 217 I 232

m/z-> 40 60 102 118 I I'l ri I 264 IXUA rp-n ■p ■i

80 100 120 140 160 180 200 220 240 260 280 I I I iT| I I I ' ' ' ' I ' ' 22.20 22.40 22.60 22.80 23.00

0522B1.D HP052902.M Wed May 29 16:40:17 2002 Page 1

NYC-WTC_000083401

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NYC-WTC_000083401Source: NYC Law Department, mirrored locally

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