VOC analysis results, sample AE11905, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\l\DATA\02MAY22\0522C10.D Vial 2 Acq On : 22 May 2002 10:35 am Operator 201-wb Sample : cal 10 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: Jun 3 14:15 2002 Quant Results File: HP051702.RES

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri May 31 11:43:42 2002 Response via : Initial Calibration DataAcq Meth : HP052102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZ ENE 15.02 114 1126593 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.69 117 1073880 5.00 ug/L -0.02 52) 1,4-DICHLOROBENZENE-D4 26.87 152 539824 5.00 ug/L -0.02

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.25 65 520930 4.74 ug/L -0.02 Spiked Amount 5.000 Recovery = 94.80% 3) 4-BROMOFLUOROBENZENE 24.28 174 438087 5.51 ug/L -0.02 Spiked Amount 5.000 Recovery = 110.20% 25) TOLUENE-D8 18.39 98 1373298 4.68 ug/L -0.02 Spiked 7\mount 5.000 Recovery = 93.60%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.81 85 373285 8.78 ug/L 99 5) CHLOROMETHANE 5.32 50 634253 9.40 ug/L 100 6) VINYL CHLORIDE 5.55 62 328060 9.57 ug/L 98 7) BROMOMETHANE 6.52 94 136616 7.93 ug/L 99 8) CHLOROETHANE 6.66 64 321439 9.54 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.21 101 585959 9.30 ug/L 100 11) 1,1,2-Trichloro-l,2,2-trif 8.11 101 349081 9.69 ug/L 96 12) ACETONE 8.19 43 246476 24.70 ug/L 97 13) 1,1-DICHLOROETHENE 8.53 61 822209 10.15 ug/L 99 14) METHYLENE CHLORIDE 9.54 49 740921 10.03 ug/L 99 15) METHYL TERT BUTYL ETHER 9.84 73 520951 9.10 ug/L 100 16) TRANS-1,2-DICHLOROETHENE 10.20 61 873548 10.64 ug/L 95 17) 1,1-DICHLOROETHANE 11.09 63 942343 10.60 ug/L 100 18) 2-BUTANONE (MEK) 11.92 43 280535 37.44 ug/L 96 19) 2,2-DICHLOROPROPANE 12.31 77 767208 10.64 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.40 96 529291 10.97 ug/L 99 21) CHLOROFORM 12.74 83 997225 10.48 ug/L 99 2 2) BROMOCHLOROMETHANE 13.11 49 402973 10.77 ug/L 96 23) 1,2-DICHLOROETHANE 14.46 62 738951 10.39 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.62 97 808997 9.27 ug/L 99 27) 1,1-DICHLOROPROPENE 13.95 75 802381 9.87 ug/L 100 28) CARBON TETRACHLORIDE 14.22 117 691077 9.62 ug/L 100 29) BENZENE 14.56 78 1749652 9.96 ug/L 100 30) TRICHLOROETHENE 15.84 95 580403 9.92 ug/L 99 31) 1,2-DICHLOROPROPANE 16.19 63 467152 9.86 ug/L 98 32) DIBROMOMETHANE 16.86 174 221476 9.65 ug/L 96 33) BROMODICHLOROMETHANE 16.70 83 665164 9.65 ug/L 98 34) 2-CHLOROETHYL VINYL ETHER 17.18 63 114625 12.55 ug/L 97 35) METHYL ISO-BUTYL KETONE 17.27 58 229767 38.71 ug/L 99 36) CIS-1,3-DICHLOROPROPENE 17.79 75 659275 9.88 ug/L 99 37) TOLUENE 18.56 91 1829822 10.21 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.83 75 477342 8.56 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.22 97 278060 10.07 ug/L 97 40) TETRACHLOROETHENE 20.01 166 558257 10.57 ug/L 98 41)■1,3-DICHLOROPROPANE 19.75 76 539229 10.06 ug/L 99 42) DIBROMOCHLOROMETHANE 20.45 129 342502 10.26 ug/L 99 43) 1,2-DIBROMOETHANE 20.89 107 280241 9.75 ug/L 99 44) CHLOROBENZENE 21.78 112 1153075 10.62 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.83 131 423613 10.11 ug/L 96 46) 2-HEXANONE 19.12 43 438052 38.56 ug/L 98 47) ETHYLBENZENE 21.81 91 2244139 10.63 ug/L 99

(#) = qualifier out of range (m) = manual integration 0522C10.D HP051702.M Mon Jun 03 14:15:11 2002 Page 1

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