VOC analysis results, sample AE10890, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\l\DATA\02MAY07\0507C10B.D . Vial: 3 Acq On 8 May 2002 3:42 am Operator: 201-wb Sample cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: May 8 9:20 2002 Quant Results File: HP042202.RES Quant Method : C:\HPCHEM\1\METHODS\HP042202.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Apr 22 14:40:13 2002 Response via : Initial Calibration DataAcq Meth : HP042202

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 1470080 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.78 117 1419136 5.00 ug/L 0.03 52) 1/4-DICHLOROBENZENE-D4 26.97 152 707978 5.00 ug/L 0.03

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 702868 5.22 ug/L 0.03 Spiked Amount 5.000 Recovery = 104.40% 3) 4-BROMOFLUOROBENZENE 24.36 174 558885 5.14 ug/L 0.03 Spiked Amount 5.000 Recovery = 102.80% 25) TOLUENE-D8 18.47 98 1800091 4.91 ug/L 0.03 Spiked Amount 5.000 Recovery = 98.20%

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.87 85 548036 9.51 ug/L 98 5) CHLOROMETHANE 5.45 50 637700 8.61 ug/L 97 6) VINYL CHLORIDE 5.60 62 482826 11.39 ug/L 99 7) BROMOMETHANE 6.59 94 427722 11.10 ug/L 96 8) CHLOROETHANE 6.73 64 439476 10.48 ug/L 96 9) TRICHLOROFLUOROMETHANE 7.30 101 721767 9.94 ug/L 99 11) l,l,2-Trichloro-l,2,2-trif 8.19 101 583044 12.05 ug/L 94 12) ACETONE 8.28 43 314433 25.14 ug/L 98 13) 1,1-DICHLOROETHENE 8.62 61 1167372 9.58 ug/L 98 14) METHYLENE CHLORIDE 9.62 49 955727 8.30 ug/L 95 15) METHYL TERT BUTYL ETHER 9.93 73 642696 8.07 ug/L 94 16) TRANS-1,2-DICHLOROETHENE 10.28 61 1149515 9.14 ug/L 98 17) 1,1-DICHLOROETHANE 11.19 63 1242069 8.91 ug/L 98 18) 2-BUTANONE (MEK) 12.02 43 349173 28.71 ug/L 94 19) 2,2-DICHLOROPROPANE 12.41 77 743817 7.37 ug/L 100 20) CIS-1,2-DICHLOROETHENE 12.50 96 703687 10.10 ug/L 96 21) CHLOROFORM 12.84 83 1323901 10.01 ug/L 99 22) BROMOCHLOROMETHANE 13.21 49 526990 8.63 ug/L 84 23) 1,2-DICHLOROETHANE 14.56 62 998093 9.80 ug/L 97 26) 1,1,1-TRICHLOROETHANE 13.72 97 1017620 9.77 ug/L 97 27) 1,1-DICHLOROPROPENE 14.05 75 1045662 9.67 ug/L 98 28) CARBON TETRACHLORIDE 14.32 117 883119 10.06 ug/L 99 29) BENZENE . 14.66 78 2297009 9.23 ug/L 99 30) TRICHLOROETHENE 15.94 95 763538 9.56 ug/L 95 31) 1,2-DICHLOROPROPANE 16.28 63 608843 8.54 ug/L 97 32) DIBROMOMETHANE 16.96 174 286277 9.35 ug/L 94 33) BROMODICHLOROMETHANE 16.80 83 877798 9.59 ug/L 100 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 169118 8.26 ug/L 99 35) METHYL ISO-BUTYL KETONE 17.37 58 310541 33.89 ug/L 97 36) CIS-1,3-DICHLOROPROPENE 17.89 75 822651 8.89 ug/L 99 37) TOLUENE 18.66 91 2351651 9.34 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.93 75 593649 8.88 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.32 97 370254 9.44 ug/L 98 40) TETRACHLOROETHENE 20.11 166 661170 9.52 ug/L 96 41) 1,3-DICHLOROPROPANE 19.85 76 728443 9.23 ug/L 98 42) DIBROMOCHLOROMETHANE 20.53 129 446309 9.87 ug/L 98 43) 1,2-DIBROMOETHANE 20.99 107 365464 9.17 ug/L 94 44) CHLOROBENZENE 21.86 112 1487988 9.81 ug/L 96 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 555770 10.08 ug/L 98 46) 2-HEXANONE 19.21 43 558998 31.98 ug/L 99 47) ETHYLBENZENE 21.91 91 2781293 9.72 ug/L 99

(#) = qualifier out of range (m) = manual integration 0507C10B.D HP042202.M Wed May 08 09:20:21 2002 Page 1

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