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Laboratory blank analysis results, sample AE10186, May 2002

Machine-extracted title · confidence 90%

Results for laboratory blank sample AE10186 analyzed between April 30 and May 2, 2002.

NYC-WTC_000082518–000082541

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

, Data File C:\MSDCHEM\l\DATA\050202\LBA0502.D Vial: 18 Acq On 2 May 2002 3:53 pm Operator: Bohlk / Inst 213 Sample LB 4/30/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050.102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 7 5,6-Dihydro-la,6-diazaphena... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

26.13 0.20 ug/L 421040 p-Terphenyl d-14 26.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5,6-Dihydro-la,6-diazaphenanthre... 212 C12H8N2O2 000000-00-0 50 2 Naphtho[2,3-b]thiophene, 4,9-dim... 212 C14H12S 016587-34-1 47 3 2,8-Dimethyldibenzo(B,D)thiophen... 212 C14H12S 001207-15-4 40 4 Silanthrene, 5,10-dihydro- (CAS)... 212 C12H12Si2 007531-42-2 39 Abundance Scan 1660 (26.133 min): LBA0502.D (-) m/z 212.20 100.00% 2 2

5000

54 78 106 395 25.80 26.00 26.20 26.40 0 - 1I 1' 1 m/z 208.20 16.40% nn/z~> 0 50 100 150 200 250 300 350 Abundance #132892; 5,6-bihydro-1 a,6-diazaphenanthren-3'5-dione 2 2 184

5000 25.80 26.00 26.20 26.40 m/z 106.10 14.36% 51 78 103 129 0 - J, ,L ,1., L,,........... m/z-> 0 50 100 150 200 250 300 350 Abundance #133707: Naphtho[2,3-b]thiophene, 4,9-dimethyl- 212

I ' ' ' ' I ' ' ' ' I 25.80 26.00 26.20 26.40 5000 m/z 102.90 12.72%

0 - 'so' 'lOO ' 150 200 Tl/z-> 0 250 300 350 Abundance #133718; 2,8-Dimethyldibenzo(B,D)thiophene S$ 2,8-Dimethyl... ........... H111 f, f,, 1 .*1 2 2 25.80 26.00 26.20 26.40 m/z 87.90 12.48% (I 5000 105

152 178 I 0- 4.^ m/z-> 0 50 100 150 200 250 300 350 25.80 26.00 26.20 26.40

LBA0502.D 050102.M Mon May 06 14:19:59 2002 Page 9

NYC-WTC_OOOO82546

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NYC-WTC_000082540Source: NYC Law Department, mirrored locally

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