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GCMS analysis results for sample AD25039, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25039 conducted on November 19, 2001, identifying unknown compounds.

NYC-WTC_000069234–000069244

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0801\25039.D Vial; 13 Acq On : 9 Nov 2001 2:19 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 135467 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 "entative ID MW MolForm CAS# Qual

1 l,4-Dichlotobenzene-d4 150 C6C12D4 003855-82-1 58 2 Benzene-/2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 Cyclop^tanone, 2-cyclopentylidene- 150 C10H14O 000825-25-2 9 4 Benzaldehyde, 2-hydroxy-5-methoxy- 152 C8H8O3 000672-13-9 9 Abundance / Scan 711 (11.572 min): 25039.D {-) ~~ m/z 149.90 100.00% 1!i0 A 5000 115 52 ™ 11.20 11.40 11.60 11.80 12.00 40 ' ' I ' ' I' I ' tAsAt 87 rA m/z 151.90 . 65.98% Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 .160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 33.30% 35 At Ti*-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 4bundance #9592; Benzene-1,2,3,4-d4-, 5,6-dichloro- liiO

115 11.20 11.40 11.60 11,80 12.00 5000 52 78 m/z78.05 19.42%

35 87

Tife-> 30 I 40 50 60 70 I 80 90 100 110 120 130 .AU.,- 140 150 160 Abundance #9841: Cyclopentanone, 2-cyclopentylidene- ........ (....... liiO 11.20 11.40 11.60 11.80 12.00 79 m/z52.00 15.17%

5000 67 94 107 122 135 f > I I I I I . I I I I > I I I I . r I I . . I I I .

T,fe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1120 1140 1160 1180 1200

25039.D NP103001.M Mon Nov 19 14:35:54 2001 Page 2

NYC-WTC_000069243

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NYC-WTC_000069243Source: NYC Law Department, mirrored locally

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