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GCMS analysis results, sample AD24876, Nov 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AD24876 performed on 11/19/2001, identifying unknown compounds with analyst notes.

NYC-WTC_000068979–000068990

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068989
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24876.D Vial: 5 Acq On : 6 Nov 2001 4:42 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 l,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.55 ug/1 95841 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-Dichloro^nzene-d4 150 C6C12D4 003855-82-1 64 2 Benzene-l,2y3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 23 3 2-Methoxy-y, 5,6-trimethylpyrimidine 152 C8H12N2O 065641-61-4 9 4 2-Methyl-y-nitroaniline 152 C7H8N2O2 000570-24-1 9

Ji. Abundance Scan 712 (11.578 min): 24876.D (-) m/z 149.90100.00% 1i>0

5000 115 78 52 11.20 11.40 11.60 11,80 12.00 40 I . 87 " I' ' 111 I ’• ''i' m/z 151.90 69.78% Tl&-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 52 78 115 JI 11.20 11.40 11.60 11.80 12.00 m/z 114.90 36.46% U-rr^T-rrrrrr- TTfe-> " 40 60 70 80 90 100 110 120 130 140 150 160 T rX T

Abundance #9592: Benzene-1,2,3,4-d4-. 5,6-dichloro- liO ■■ 'T'-' --rf J ' 115 11.20 11.40 11.60 11.80 12.00 5000- 52 78 m/z 78.05 21.92%

35 87 ' I ‘ I ' I ‘ ‘ ' I ’ ' ' ’ I ' ' ’ ' H ’ I ' I I •nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10194:2-Methoxy-4,5,6-trimethylpyrimidine 1?2 1$2 11.20 11^40 ItTO 'I'lW 1Z(» m/z 52.10, 13.97%

5000- 52 67 107 I 98 I ‘ ‘ ‘ ‘ I 137 I ' ‘ ‘ ' I T mZz-> 3o " 4o " sb' M 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24876.D NP103001.M Mon Nov 19 10:10:42 2001 Page 3

NYC-WTC_000068989

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NYC-WTC_000068989Source: NYC Law Department, mirrored locally

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