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Document / 13 pages

GCMS sample extraction log table, Nov 2001

Machine-extracted title · confidence 85%

Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

NYC-WTC_000068400–000068412

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068408
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\LB.D Vial: 9 Acq On : 2 Nov 2001 10:50 pm Operator: 209 GALOS Sample : 10/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.55 0.61 ug/1 92439 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H14O 000623-37-0 83 2 3-Pentan,61, 2-methyl- 102 C6H14O 000565-67-3 38 3 Amylene/Hydrate 88 C5H12O 000075-85-4 36 4 4-Heptanol 116 C7H16O 000589-55-9 10 Abundance / Scan 164 6.548 min): LB.D (-) m/z 5^705 100.00% 53

5000 73

41 I , I , I , I /n (I pYpYp 11)

53 6.20 6.40 6.60 6.80 85 1" ' • 1 ‘ 'I 11111 u ' I" " 1" '' I''" I " " I " " I " " I' m/z 55700 77714% nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528:3-Hexanol 519

73 5000 M ' ' ' ' I ' ' ' ' I ' ' ' ' i ' 31 6.20 6.40 6.60 6.80 m/z 73.00 46.98% 45 84 fn-n-p-rTTp4 +4 'I'"....... I I " ‘' I'''' I'''' I p" Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561:3-Pentanol, 2-methyl- 59 . .............................. , , ,.p 6.20 6.40 6.60 6.80 WMW 73 “mTz 41.05 22.56% 31 45 85 102 ... " I" "I" "I I".. . ' I'''' I" '' I " '' I' " ' I'' " I'''' I'''' I' •nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #849: Amylene Hydrate 519 6.20 6.40 6.60 6.80 m/z 42.95 22.26% 73 31

Ti/z-> #,44™^ l""l'l"llllll 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 1'''' I " '' I' " ' I “ “ I " '' I r 6.20 JVJ I ' ' ' ' I 6.40 6.60 6.80 ■p

LB.D NP103001.M Wed Nov 07 13:12:36 2001 Page 3

NYC-WTC_000068408

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NYC-WTC_000068408Source: NYC Law Department, mirrored locally

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