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GCMS analysis results for sample AD24219, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24219 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068037–000068054

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0101\24218.D Vial: 5 Acq On 1 Nov 2001 6:55 pm Operator: 209 GALOS Sample : gc/ms unknown Inst J GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.318 135 139 146 rBV 28284 58782 1.39% 0.265% 2 6.428 147 151 161 rW 39281 118866 2.80% 0.536% 3 6.557 161 165 173 rW 25231 65952 1.56% 0.298% 4 6.667 174 177 193 rVB 31400 82049 1.94% 0.370% 5 7.695 285 289 295 rBV 103192 254926 6.01% 1.150% 6 11.579 706 712 721 rBV 32367 78993 1.86% 0.356% 7 11.716 721 727 750 rW 1138411 2977498 70.24% 13.434% 8 15.315 1114 1119 1137 rBV 1850697 4090304 96.49% 18.455% 9 20.594 1688 1694 1715 rBV 1961653 4239250 100.00% 19.127% 10 25.019 2169 2176 2189 rBV2 1921956 4046722 95.46% 18.259% 11 33.061 3045 3052 3071 rBV2 1379762 3267790 77.08% 14.744% 12 37.155 3489 3498 3512 rBV 928885 2549467 60.14% 11.503% 13 38.064 3589 3597 3602 rBV4 12668 46772 1.10% 0.211% 14 39.634 3759 3768 3779 rBV4 17368 87143 2.06% 0.393% 15 41.580 3969 3980 3987 rBV3 18276 101321 2.39% 0.457%

16 44.031 4235 4247 4258 rBV7 13026 97471 2.30% 0.440%

Sum of corrected areas: 22163306 24218.D NP103001.M Tue Nov 06 11:48:23 2001

NYC-WTC_000068043

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NYC-WTC_000068043Source: NYC Law Department, mirrored locally

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