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GCMS analysis results, sample AD25461, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25461 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069659–000069675

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV1601\25461.D Vial: 3 Acq On : 16 Nov 2001 4:59 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.701 285 289 306 rBV 65843 220564 4.43% 0.808% 2 11.712 721 726 747 rBV 1319878 3444653 69.13% 12.613% 3 15.320 1113 1119 1137 rBV 2099621 4569231 91.70% 16.731% 4 20.599 1687 1694 1715 rBV 2225050 4982743 100.00% 18.245% 5 25.015 2169 2175 2188 rBV2 2152123 4809500 96.52% 17.611%

6 25.162 2188 2191 2205 rVB 17691 54235 1.09% 0.199% 7 33.057 3044 3051 3073 rBV2 1848153 4325143 86.80% 15.837% 8 36.747 3447 3453 3463 rBV 29750 93699 1.88% 0.343% 9 37.151 3488 3497 3522 rBV2 1323716 3894629 78.16% 14.261% 10 38.060 3588 3596 3606 rBV2 37526 151492 3.04% 0.555%

11 39-.639 3759 3768 3779 rBV2 39529 198999 3.99% 0.729% 12 41.594 3967 3981 3997 rBV4 38415 248263 4.98% 0.909% 13 44.045 4232 4248 4263 rBV5 26345 214309 4.30% 0.785% 14 47.130 4566 4584 4587 rBV6 16231 102124 2.05% 0.374%

Sum of corrected areas: 27309584

25461.D NP103001.M Wed Nov 21 11:43:15 2001

NYC-WTC_000069665

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NYC-WTC_000069665Source: NYC Law Department, mirrored locally

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