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GCMS analysis results for sample AD24218, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24218 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068022–000068036

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0101\24217.D Vial: 4 Acq On : 1 Nov 2001 5:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise • : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.314 134 138 144 rBV 20758 46111 1.21% 0.226% 2 6.415 146 149 160 rW 32698 96270 2.52% 0.471% 3 6.544 160 163 172 rW 18145 49777 1,30% 0.244% 4 6.663 172 176 187 rVB 24654 57577 1.51% 0.282% 5 7.682 284 287 293 rBV 83396 206015 5.39% 1.008%

6 C^664 390 394 406 rBV 27005 73009 1.91% 0.357% 7 117-5^ 707 711 720 rVB2 29678 77694 2.03% 0.380% 8 712 720 726 746 rBV 1059682 2716692 71.13% 13.291% 9 -2.19,. 773 778 794 rBV2 55000 225292 5.90% 1.102% 10 15.320 1113 1119 1135 rBV 1797886 3706052 97.04% 18.132% 11 20.599 1687 1694 1705 rBV 1778974 3819107 100.00% 18.685% 12 25.015 2169 2175 2188 rBV2 1622604 3636494 95.22% 17.792% 13 33.057 3044 3051 3062 rBV2 1348469 3117721 81.63% 15.253% 14 37.151 3489 3497 3515 rBV2 942360 2611678 68.38% 12.778%

Sum of corrected areas: 20439489 24217.D NP103001.M Tue Nov 06 11:46:39 2001

NYC-WTC_000068028

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NYC-WTC_000068028Source: NYC Law Department, mirrored locally

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