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GCMS analysis results for sample AD23998, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23998 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067796–000067810

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\OCT2501\23998.D Vial: 6 Acq On : 25 Oct 2001 5:35 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.367 140 144 150 rBV 54299 105283 1.73% 0.353% 2 6.468 151 155 166 rW 85924 204576 3.37% 0.686% 3 6.605 166 170 178 rW 42021 87692 1.44% 0.294% 4 6.715 178 182 194 rVB 56207 117376 1.93% 0.394% 5 7.725 288 292 307 rBV 167103 370812 6.11% 1.243% 6 11.590 709 713 723 rBV 51573 106858 1.76% 0.358% 7 11.728 723 728 748 rBV 1761009 4103171 67.59% 13.758% 8 15.345 1115 1122 1138 rBV 2486180 5822655 95.91% 19.523% 9 20.633 1689 1698 1712 rBV 2620181 6071119 100.00% 20.356% 10 25.067 2172 2181 2192 rBV2 2519081 5768187 95.01% 19.341% 11 33.100 3048 3056 3078 rBV2 1685336 4044894 66.63% 13.562% 12 37.203 3495 3503 3522 rBV2 1039884 3021690 49.77% 10.132%

Sum of corrected areas: 29824313 23998.D NP101901.M Fri Oct 26 10:12:10 2001

NYC-WTC_000067802

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NYC-WTC_000067802Source: NYC Law Department, mirrored locally

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