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GCMS analysis results for sample AD24046, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24046 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067811–000067825

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\OCT2501\24046.D Vial: 7 Acq On : 25 Oct 2001 6:33 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.359 139 143 150 rBV 44719 90460 1.65% 0.328% 2 6.460 150 154 165 rW 72912 173949 3.18% 0.630% 3 6.598 165 169 177 rW 33723 78099 1.43% 0.283% 4 6.708 177 181 190 rVB 46135 102079 1.87% 0.370% 5 7.718 288 291 303 rBV 125082 301526 5.51% 1.092% 6 11.592 707 713 723 rBV 45489 106229 1.94% 0.385% 7 11.739 723 729 742 rBV 1536216 3688852 67.42% 13.360% 8 15.346 1115 1122 1138 rBV 2351972 5205930 95.14% 18.855% 9 20.634 1690 1698 1711 rBV 2425619 5471626 100.00% 19.817% 10 25.059 2173 2180 2190 rBV2 2388992 5192034 94.89% 18.804% 11 33.101 3048 3056 3073 rBV2 1699683 3966517 72.49% 14.366% 12 37.205 3494 3503 3522 rBV2 1100826 3233463 59.10% 11.711%

Sum of corrected areas: 27610764 24046.D NP101901.M Fri Oct 26 12:18:47 2001

NYC-WTC_000067817

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NYC-WTC_000067817Source: NYC Law Department, mirrored locally

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