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GCMS analysis results for sample AD24480, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24480 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068529–000068543

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C;\HPCHEM\1\DATA\NOV0201\24480 .D Vial: 18 Acq On : 3 Nov 2001 7:34 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.312 134 138 144 rBV 31400 63135 1.58% 0.297% 2 6.422 146 150 161 rW 44976 139379 3.49% 0.656% 3 6.550 161 164 169 rW 27240 60324 1.51% 0.284% 4 6.661 173 176 192 rVB 33590 88216 2.21% 0.415% 5 7.156 223 230 235 rBV 16210 54731 1.37% 0.257%

6 7.689 285 288 304 rBV 58587 176847 4.43% 0.832% 7 11.572 707 711 721 rBV 28523 70363 1.76% 0.331% 8 11.710 721 726 743 rBV 1076042 2751262 68.94% 12.944% 9 15.318 1113 1119 1137 rBV 1761901 3760335 94.22% 17.691% 10 20.596 1687 1694 1707 rBV 1855565 3990866 100.00% 18.775% 11 25.021 2169 2176 2185 rBV 1772912 3780393 94.73% 17.785% 12 33.054 3044 3051 3070 rBV2 1488072 3460877 86.72% 16.282% 13 37.158 3490 3498 3511 rBV 1008982 2859070 71.64% 13.451%

Sum of corrected areas: 21255798 24480.D NP103001.M Tue Nov 13 10:12:42 2001

NYC-WTC_000068535

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NYC-WTC_000068535Source: NYC Law Department, mirrored locally

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