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GCMS analysis results for sample AD24488, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068585–000068597

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File ; C:\HPCHEM\1\DATA\NOV0501\24488.D Vial: 6 Acq On 5 Nov 2001 4:50 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 6.327 / 136 140 146 rBV 29727 59159 1.15% 0.225% 2 6.428 / 146 151 162 rW 45347 123617 2.41% 0.471% 3 6.556^ 162 165 172 rW 24666 58178 1.13% 0.222% 4 6.676 ■' 174 178 195 rVB 31349 83591 1.63% 0.318% 5 7.695 0 285 289 307 rBV 104584 286912 5.59% 1.093%

6 11.578^ 707 712 37274 721 rBV 92328 1.80% 0.352% 7 11.707-' 721 726 1355858 746 rW 3446792 67.14% 13.128% 8 15.324-' 1113 1120 1136 rBV 2067896 4662543 90.83% 17.759% 9 20.602^ 1688 1695 1719 rBV 2257685 5133506 100.00% 19.552% 10 25.018' 2170 2176 2190 rBV2 2227704 4942203 96.27% 18.824%

11 33.060^ 3045 3052 3072 rBV2 1751854 4104774 79.96% 15.634% 12 37.164/ 3490 3499 3513 rBV 1183813 3261441 63.53% 12.422%

Sum of corrected areas: 26255044 24488.D NP103001.M Fri Nov 09 12:11:05 2001

NYC-WTC_000068591

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NYC-WTC_000068591Source: NYC Law Department, mirrored locally

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