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GCMS analysis results for sample AD24236, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24236 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068070–000068084

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data Pile : C:\HPCHEM\1\DATA\NOV0101\24220.D Vial: 7 Acq On : 1 Nov 2001 8:52 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge <100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.790 72 81 83 rBV2 19599 51609 1.14% 0.209% 2 6.322 135 139 147 rBV 27714 58363 1.29% 0.237% 3 6.423 147 150 161 rVV2 41370 108146 2.39% 0.438% 4 6.561 161 165 173 rVB 22986 54741 1.21% 0.222% 5 6.671 173 177 184 rBV 30676 66670 1.47% 0.270% 6 7.158 225 230 237 rBV 14641 46864 1.04% 0.190% 7 7.690 285 288 295 rBV 88726 212840 4.70% 0.863% 8 8.673 390 395 416 rBV 31810 92471 2.04% 0.375% 9 11.574 702 711 720 rBV 37853 96393 2.13% 0.391% 10 11.711 720 726 746 rBV 1283362 3146895 69.56% 12.754% 11 15.319 1113 1119 1137 rBV 2058538 4411764 97.52% 17.881% 12 20.598 1687 1694 1717 rBV 2158246 4523728 100.00% 18.334% 13 25.023 2169 2176 2188 rBV 2047229 4383631 96.90% 17.767% 14 33.055 3044 3051 3076 rBV2 1735939 4036393 89.23% 16.359% 15 37.159 3489 3498 3513 rBV2 1199199 3382985 74.78% 13.711%

Sum of corrected areas: 24673493 24220.D NP103001.M Tue Nov 06 11:51:03 2001

NYC-WTC_000068076

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NYC-WTC_000068076Source: NYC Law Department, mirrored locally

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