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GCMS analysis results for sample AD24217, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24217 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068003–000068021

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0101\24216.D Vial: 3 Acq On : 1 Nov 2001 4:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.313 134 138 144 rBV 24961 50786 1.02% 0.188% 2 6.414 146- 149 159 rVV2 39830 100243 2.01% 0.371% 3 6.552 160 164 172 rW 21730 51854 1.04% 0.192% 4 6.662 172 176 185 rW 26035 56921 1.14% 0.211% 5 7.690 284 288 293 rBV 87142 208660 4.19% 0.772%

6 11.573 707 711 720 rBV 35582 88213 1.77% 0.327% 7 11.711 720 726 750 rW 1330506 3326239 66.72% 12.312% 8 15.319 1113 1119 1136 rBV 2212772 4635372 92.98% 17.157% 9 20.598 1687 1694 1710 rBV 2344618 4985265 100.00% 18.452% 10 25.022 2169 2176 2187 rBV 2190989 4744819 95.18% 17.562% 11 33.055 3044 3051 3068 rBV2 1877050 4416578 88.59% 16.347% 12 33.331 3074 3081 3089 rVB 40713 91127 1.83% 0.337% 13 35.066 3266 3270 3281 rBV 24798 66869 1.34% 0.248% 14 36.076 3376 3380 3383 rBV 27459 62085 1.25% 0.230% 15 36.131 3383 3386 3398 rVB 29914 90180 1.81% 0.334%

16 37.159 3488 3498 3513 rBV2 1334058 3818550 76.60% 14.134% 17 40.904 3891 3906 3916 rBV9 18303 139936 2.81% 0.518% 18 41.951 4009 4020 4033 rBV2 14552 83365 1.67% 0.309%

Sum of corrected areas: 27017062 24216.D NP103001.M Tue Nov 06 11:45:30 2001

NYC-WTC_000068008

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NYC-WTC_000068008Source: NYC Law Department, mirrored locally

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