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GC/MS analysis report for sample AD22545, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22545 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086933–000086948

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\SEP2501\22545.D Vial: 11 Acq On : 26 Sep 2001 12:15 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.388 144 147 155 rBV 22990 51276 1.47% 0.281% 2 6.498 155 159 163 rBV 31578 65967 1.90% 0.361% 3 6.627 169 173 182 rW 18442 38937 1.12% 0.213% 4 6.746 182 186 194 rVB 19363 39857 1.15% 0.218% 5 7.774 295 298 303 rBV 33985 72654 2.09% 0.398%

6 11.648 716 720 729 rVB 27485 66718 1.92% 0.365% 7 11.786 729 735 747 rW 998923 2453326 70.56% 13.426% 8 15.403 1122 1129 1145 rBV 1491020 3365183 96.78% 18.416% 9 18.065 1414 1419 1424 rBV 19159 36847 1.06% 0.202% 10 20.682 1697 1704 1721 rBV 1581547 3477080 100.00% 19.028% 11 25.116 2179 2187 2198 rBV2 1468216 3215026 92.46% 17.594% 12 27.108 2399 2404 2408 rBV 41667 77706 2.23% 0.425% 13 29.780 2690 2695 2702 rBV 83343 162868 4.68% 0.891% 14 31.772 2907 2912 2917 rVV2 29843 41118 1.18% 0.225% 15 31.900 2921 2926 2931 rVB 30545 63160 1.82% 0.346%

16 33.158 3052 3063 3074 rBV2 1092405 2651254 76,25% 14.509% 17 33.415 3086 3091 3098 rVB 24424 52185 1.50% 0.286% 18 37.271 3503 3511 3524 rBV2 809717 2342464 67.37% 12.819%

Sum of corrected areas: 18273626

22545.D NP091101.M Wed Oct 03 15:09:21 2001

NYC-WTC_000086939

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NYC-WTC_000086939Source: NYC Law Department, mirrored locally

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