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GC/MS analysis report for sample AD22544, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22544 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086913–000086932

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\SEP2501\22544.D Vial: 10 Acq On : 25 Sep 2001 11:15 pm Operator: 209 . GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.396 144 148 155 rBV 17350 37591 1.12% 0.215% 2 6.497 155 159 162 rBV 30101 58595 1.74% 0.335% 3 6.745 182 186 192 rBV 21060 43680 1.30% 0.250% 4 7.764 293 297 303 rBV 62006 140923 4.19% 0.806% 5 11.647 715 72 0 729 rVB 26950 63800 1.90% 0.365% 6 11.785 729 735 751 rBV' 981459 2407339 71.55% 13.768% 7 15.402 1122 1129 1145 rBV 1429064 3287432 97.71% 18.802% 8 20.681 1697 1704 1722 rBV 1512547 3364469 100.00% 19.242% 9 25.115 2180 2187 2199 rBV 1460493 3068790 91.21% 17.551% 10 31.771 2907 2912 2916 rW 25303 50792 1.51% 0.290% 11 32.762 3014 3020 3025 rBV 28145 56768 1.69% 0.325% 12 33.157 3055 3063 3078 rBV2 1068787 2524308 75.03% 14.437% 13 33.717 3120 3124 3130 rVB2 30363 63053 1.87% 0.361% 14 34.644 3220 3225 3230 rVB 22270 47075 1.40% 0.269% 15 35.525 3318 3321 3327 rVB 17848 36229 1.08% 0.207% 16 37.270 3502 3511 3523 rBV2 793928 2234066 66.40% 12.777%

Sum of corrected areas: 17484910

■ 22544.D NP091101.M Mon Oct 01 12:58:53 2001

NYC-WTC_OO6O8692O

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NYC-WTC_000086920Source: NYC Law Department, mirrored locally

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