GCMS reference results for sample AE06633, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR16O2\REF1.D Vial: 4 Acq On : 16 Apr 2002 4:07 pm Operator: Sample : gc/ms scan 3/22 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 11:50 2002 <Quant Results File: GCMS0412.RES

■Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. QIon_ Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 536688 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1940654 20.00 ug/1 -0.03 17) Acenaphthene-dlO 21.15 164 1101957 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.59 188 1581907 20.00 ug/1 -0.02 39) Chrysene-dl 2 33.65 240 1009514 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 635901 20.00 ug/1 -0.05

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 81148 4.41 ug/mL 0.16 Spiked Amount 5.000 Recovery = 88.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.86 74 86606 7.41 ug/1 98 3) bis(2-Chloroethyl)ether 11.61 93 212797 11.71 ug/1 98 4) 1,3-Dichlorobenzene 12.11 146 139481 7.44 ug/1 98 5) 1,4-Dichlorobenzene 12.26 146 152216 8.07 ug/1 99 6) 1,2-Dichlorobenzene 12.77 146 158650 9.06 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.09 45 288565 11.49 ug/1 99 8) N-Nitroso-di-n-propylamine 13.48 70 133165 11.17 ug/1 98 9) Hexachloroethane 13.62 117 29122 4.21 ug/1 90 11) Nitrobenzene 13.89 77 181989 10.70 ug/1 97 12) Isophorone 14.54 82 366363 11.38 ug/1 98 13) bis(2-Chloroethoxy)methane 15.22 93 251860 12.01 ug/1 99 14) 1,2,4-Trichlordbenzene 15.73 180 144081 9.77 ug/1 99 15) Naphthalene 15.90 128 541643 11.61 ug/1 99 16) Hexachlorobutadiene 16.45 225 22551 3.06 ug/1 97 18) Hexachlorocyclopentadiene 18.64 237 5312 1.09 ug/1 96 19) 2-Chloronaphthalene 19.41 162 337082 11.60 ug/1 97 20) Dimethylphthalate 20.49 163 450736 13.45 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 88035 10.99 ug/1 96 22) Acenaphthylene 20.67 152 520378 12.80 ug/1 99 23) Acenaphthene 21.24 153 365465 12.64 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 111085 10.53 ug/1 99 25) Diethylphthalate 22.63 149 426714 13.28 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 191282 13.41 ug/1 97 27) Fluorene 22.76 166 402237 13.14 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.24 , 77 359643 10.58 ug/L 97 31) N-Nitrosodiphenylamine 23.17 168 139662 10.61 ug/1 98 32) 4-Bromophenyl-phenylether 24.24 248 106272 13.84 ug/1 95

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0412.M Wed Apr 17 11:50:57 2002 Page 1

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