GCMS reference standard results for sample AE06981, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : ■C:\HPCHEM\1\DATA\APR18O2\REF1.D Vial: 6 Acq On : 18 Apr 2002 4:51 pm Operator: Sample : GC/MS SCAN 3/25 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 8:42 2002 ।Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 588754 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 2148717 20.00 ug/1 -0.03 17) Acenaphthene-dlO 21.15 164 1203123 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.59 188 1777650 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 1159101 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 726902 20.00 ug/1 -0.05 System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 84499 4.08 ug/mL 0.17 Spiked Amount 5.000 Recovery = .81.60% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.86 74 82951 6.47 ug/1 93 3) bis(2-Chloroethyl)ether 11.61 93 212788 10.67 ug/1 99 4) 1,3-Dichlorobenzene 12.11 146 183306 8.91 ug/1 98 5) 1,4-Dichlorobenzene 12.26 146 190416 9.20 ug/1 98 6) 1,2-Dichlorobenzene 12.77 146 187136 9.74 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.09 45 286044 10.38 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 133330 10.19 ug/1 98 9) Hexachloroethane 13.63 117 53142 7.01 ug/1 93 11) Nitrobenzene 13.89 77. 190857 10.13 ug/1 99 12) Isophorone 14.54 82 350820 9.84 ug/1 98 13) bis(2-Chloroethoxy)methane 15.22 93 262348 11.30 ug/1 100 14) 1,2,4-Trichlorobenzene 15.74 180 172855 10.58 ug/1 98 15) Naphthalene 15.90 128 592008 11.46 ug/1 100 16) Hexachlorobutadiene 16.44 225 60543 7.41 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 6680 1.26 ug/1 # 95 19) 2-Chloronaphthalene 19.41 162 379753 11.97 ug/1 98 20) Dimethylphthalate 20.49 163 489945 13.39 ug/1 98 21) 2,6-Dinitrotoluene 20.71 165 95061 10.87 ug/1 98 22) Acenaphthylene 20.68 152 542358 12.22 ug/1 100 23) Acenaphthene 21.24 153 395996 12.55 ug/1 98 24) 2,4-Dinitrotoluene 21.88 165 117974 ,10.25 ug/1 97 25) Diethylphthalate 22.63 149 466782 13.30 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 221337 14.22 ug/1 98 27) Fluorene 22.76 166 447961 13.41 ug/1 97 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 396729 10.68 ug/L 95 31) N-Nitrosodiphenylamine 23.17 168 133170 9.01 ug/1 98 32) 4-Bromophenyl-phenylether 24.25 248 122545 14.20 ug/1 95 (#) = qualifier out of range (m) = manual integration REFl.D GCMS0412.M Fri Apr 19 08:45:26 2002 Page 1

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