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GCMS unknown compound analysis, sample AE05308, March 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05308 conducted on March 29, 2002, identifying unknown compounds.

NYC-WTC_000059399–000059409

Folder label: “GCMS X 3/11/02 A 3/17/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\031702\5308FB.D Vial: 11 Acq On : 17 Mar 2002 4:58 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.570 271 275 288 rBV 128793 411900 4.52% 0.699% 2 9.543 709 713 732 rBV 2113647 5926822 65.09% 10.054% 3 12.056 ■ 985 990 999 rBV 738540 1372999 15.08% 2.329% 4 13.026 1091 1097 1119 rBV 3967065 8381408 92.04% 14.217% 5 18.133 1654 1660 1679 rBV 4482713 8992841 98.76% 15.255%

6 22.496 2135 2141 2155 rBV2 4119206 9106073 100.00% 15.447% 7 22.650 2155 2158 2167 rVB2 33739 112644 1.24% 0.191% 8 24.645 2374 2378 2388 rBV 38422 99632 1.09% 0.169% 9 27.430 2680 2685 2700 rBV 721350 1416906 15.56% 2.404% 10 30.305 2995 3002 3024 rBV2 3826952 8713737 95.69% 14.781%

11 33.380 3334 3341 3368 rBV 3338214 8755719 96.15% 14.852% 12 34.178 3422 3429 3449 rBV2 2187958 5660805 62.17% 9.602%

Sum of corrected areas: 58951486

;308FB.D 5080302.M Mon Mar 25 06:51:24 2002 Page 1

NYC-WTC_000059404

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NYC-WTC_000059404Source: NYC Law Department, mirrored locally

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