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GCMS unknown compound analysis, sample AE05303, March 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05303 conducted on March 29, 2002, identifying unknown compounds.

NYC-WTC_000059460–000059470

Folder label: “GCMS X 3/11/02 A 3/17/02

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Scanned page image, NYC-WTC_000059465
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\031702\5303.D Vial: 6 Acq On : 17 Mar 2002 12:53 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 272 274 293 rBV 127134 465019 5.17% 0.929% 2 9.543 708 713 731 rBV 2117015 5897599 65.61% 11.785% 3 12.047 985 989 998 rBV2 114748 214370 2.38% 0.428% 4 13.026 1091 1097 1113 rBV 3896133 8270023 92.01% 16.526% 5 18.133 1654 1660 1679 rBV 4436159 8876522 98.75% 17.738%

6 22.495 2134 2141 2155 rBV2 4013032 8988504 100.00% 17.962% 7 24.645 2374 2378 2394 rBV 56694 137556 1.53% 0.275% 8 27.430 2680 2685 2693 rBV 798535 1530275 17.02% 3.058% 9 30.305 2995 3002 3019 rBV2 3774380 8841336 98.36% 17.668% 10 30.613 3030 3036 3050 rVB 275626 653373 7.27% 1.306%

11 34.178 3422 3429 3442 rBV2 2457893 6168114 68.62% 12.326%

Sum of corrected areas: 50042691

5303.D 5080302.M Fri Mar 22 09:42:42 2002 Page 1 ■

NYC-WTC_000059465

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NYC-WTC_000059465Source: NYC Law Department, mirrored locally

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