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GCMS unknown compound analysis, sample AE05514, March 2002

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Laboratory report documenting GCMS analysis of sample AE05514 conducted on March 29, 2002, identifying unknown compounds.

NYC-WTC_000059440–000059449

Folder label: “GCMS X 3/11/02 A 3/17/02

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Scanned page image, NYC-WTC_000059445
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\031702\5514.D Vial: 15 Acq On : 17 Mar 2002 8:13 pm Operator: McLean Sample : 3/11/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 271 274 292 rBV 105655 398876 5.06% 0.916% 2 9.543 708 713 737 rBV 1668251 5075489 64.33% 11.660% 3 12.047 985 989 1002 rBV 305207 557821 7.07% 1.281% 4 13.017 1091 1096 1112 rBV 3278936 7076354 89.69% 16.256% 5 18.133 1654 1660 1676 rBV 3872088 7799495 98.86% 17.917%

6 22.496 2135 2141 2155 rBV2 3405403 7889662 100.00% 18.125% 7 22.659 2155 2159 2165 rVB3 26203 89046 1.13% 0.205% 8 27.430 2680 2685 2697 rBV 632593 1221645 15.48% 2.806% 9 30.305 2995 3002 3025 rBV2 3309239 7808451 98.97% 17.938% 10 34.178 3422 3429 3448 rBV2 2246356 5613253 71.15% 12.895%

Sum of corrected areas: 43530092

5514.D 5080302.M Mon Mar 25 06:55:04 2002 Page 1

NYC-WTC_000059445

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NYC-WTC_000059445Source: NYC Law Department, mirrored locally

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