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GCMS unknown compound analysis, sample AE05305, March 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis of sample AE05305 conducted on 3/29/2002, testing for unknown organic compounds.

NYC-WTC_000059379–000059388

Folder label: “GCMS X 3/11/02 A 3/17/02

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Scanned page image, NYC-WTC_000059384
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\031702\5305.D Vial: 8 Acq On : 17 Mar 2002 2:31 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 271 274 279 rBV 147517 346963 3.91% 0.728% 2 9.543 708 713 730 rBV 2099456 5797136 65.28% 12.159% 3 12.056 985 990 997 rBV 151265 280018 3.15% 0.587% 4 13.026 1091 1097 1110 rBV 3883179 8118916 91.43% 17.029% 5 18.133 1654 1660 1685 rBV 4373370 8814047 99.25% 18.487%

6 22.495 2134 2141 2154 rBV2 3949905 8880223 100.00% 18.626% 7 22.650 2154 2158 2166 rVB2 33547 119528 1.35% 0.251% 8 27.430 2681 2685 2694 rBV 778823 1504974 16.95% 3.157% 9 30.305 2995 3002 3021 rBV2 3639014 8539130 96.16% 17.911% 10 30.913 3064 3069 3079 rVB 46639 117279 1.32% 0.246%

11 34.178 3422 3429 3442 rBV2 2123663 5157644 58.08% 10.818%

Sum of corrected areas: 47675858

;305.D 5080302.M Mon Mar 25 06:48:17 2002 Page 1

NYC-WTC_000059384

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NYC-WTC_000059384Source: NYC Law Department, mirrored locally

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