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GCMS unknown compound analysis, sample AE05513, March 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05513 conducted on March 29, 2002, identifying unknown compounds.

NYC-WTC_000059430–000059439

Folder label: “GCMS X 3/11/02 A 3/17/02

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Scanned page image, NYC-WTC_000059435
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C;\MSDCHEM\l\DATA\031702\5513Q.D Vial: 14 Acq On : 17 Mar 2002 7:24 pin Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 271 274 289 rBV 106763 383273 4.45% 0.820% 2 9.543 708 713 734 rBV 1889382 5583130 64.81% 11.945% 3 12.046 985 989 996 rBV2 193303 354915 4.12% 0.759% 4 13.026 1091 1097 1119 rBV 3631999 7880780 91.49% 16.861% 5 18.133 1654 1660 1681 rBV 4223610 8522271 98.93% 18.233%

6 22.495 2135 2141 2155 rBV2 3809837 8614178 100.00% 18.430% 7 22.649 2155 2158 2172 rVB3 37036 141903 1.65% 0.304% 8 27.430 2680 2685 2698 rBB 770298 1511242 17.54% 3.233% 9 30.305 2995 3002 3024 rBV2 3578965 8327477 96.67% 17.817% 10 34.178 3422 3429 3449 rBV2 2190130 5421031 62.93% 11.598%

Sum of corrected areas: 46740200

5513Q.D 5080302.M Mon Mar 25 06:54:15 2002 Page 1

NYC-WTC_000059435

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NYC-WTC_000059435Source: NYC Law Department, mirrored locally

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