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GCMS surrogate recovery data, sample AE04383, April 2, 2002

Machine-extracted title · confidence 100%

Laboratory record from April 2, 2002 documenting the recovery of surrogate standards for sample AE04383.

NYC-WTC_000012486–000012493

Folder label: “GCMS X 3-1-02 A 3-27-02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\032602\4383.D Vial: 36 Acq On : 27 Mar 2002 10:09 am Operator: McLean Sample : SAMPLE 4383 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 9.548 1094 1101 1125 rBV 2950651 7477691 62.49% 12.475% 2 13.027 1685 1693 1716 rBV 5422763 11090937 92.68% 18.503% 3 18.138 2553 2563 2585 rBV 5614100 11966767 100.00% 19.964% 4 22.498 3295 3305 3326 rBV2 5099294 11852704 99.05% 19.774% 5 22.645 3326 3330 3342 rVB4 51381 146337 1.22% 0.244% 6 24.643 3663 3670 3683 rBV 249634 571868 4.78% 0.954% 7 27.428 4137 4144 4158 rBV2 675781 1373662 11.48% 2.292% 8 30.313 4624 4635 4653 rBV2 3834371 9404488 78.59% 15.690% 9 30.918 4731 4738 4749 rBV3 92067 247040 2.06% 0.412% 10 34.185 5283 5294 5319 rBV2 2252868 5809458 48.55% 9.692%

Sum of corrected areas: 59940952

1383.D 5080302.M Wed Mar 27 11:51:27 2002 Page 1

NYC-WTC_000012491

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NYC-WTC_000012491Source: NYC Law Department, mirrored locally

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