GCMS analysis report, sample AE04377, April 2, 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\032602\4377.D Vial: 30 Acq On : 27 Mar 2002 5:12 am Operator: McLean Sample : SAMPLE 4377 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.548 1094 1101 1122 rBV 2770455 6853717 66.90% 13.236% 2 9.830 1145 1149 1166 rVB8 34371 115306 1.13% 0.223% 3 12.051 1521 1527 1535 rBV 123811 200825 1.96% 0.388% 4 13.027 1684 1693 1715 rBV 4759847 9718644 94.87% 18.769% 5 18.138 2553 2563 2586 rBV 4939627 10244418 100.00% 19.784%

6 22.498 3295 3305 3323 rBV2 4177460 9561936 93.34% 18.466% 7 24.649 3665 3671 3682 rBV 64185 153327 1.50% 0.296% 8 27.434 4137 4145 4156 rBV 654791 1282541 12.52% 2.477% 9 30.307 4624 4634 4652 rBV2 3555953 8348789 81.50% 16.123% 10 34.185 5282 5294 5315 rBV2 2065066 5301224 51.75% 10.238%

Sum of corrected areas: 51780727

4377.D 5080302.M Wed Mar 27 09:10:23 2002 Page 1

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