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GCMS unknown compound analysis, sample AE05309, March 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05309 conducted on March 29, 2002, identifying unknown compounds.

NYC-WTC_000059410–000059419

Folder label: “GCMS X 3/11/02 A 3/17/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

- Data File : C:\MSDCHEM\l\DATA\031702\5309FB.D Vial: 12 Acq On : 17 Mar 2002 5:46 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

-peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 271 274 292 rBV 112226 395193 5.04% 0.933% 2 9.543 709 713 738 rBV 1690045 5059850 64.52% 11.941% 3 12.056 985 990 1001 rBV2 163583 300933 3.84% 0.710% 4 13.026 1091 1097 1120 rBV 3268682 7208637 91.92% 17.012% 5 18.133 1654 1660 1675 rBV 3844991 7737865 98.67% 18.260%

6 22.495 2135 2141 2155 rBV2 3374331 7842164 100.00% 18.507% 7 24.645 2374 2378 2391 rBV 42649 114512 1.46% 0.270% 8 27.430 2680 2685 2697 rBV 635132 1230063 15.69% 2.903% 9 30.305 2995 3002 3024 rBV2 3264426 7666456 97.76% 18.092% 10 34.178 3422 3429 3452 rBV 1985032 4819307 61.45% 11.373%

Sum of corrected areas: 42374980

5309FB.D 5080302.M Mon Mar 25 06:52:17 2002 Page 1

NYC-WTC_000059415

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NYC-WTC_000059415Source: NYC Law Department, mirrored locally

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