GCMS calibration results, sample AE05035, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR3002\REF2.D Vial: 18 Acq On : 30 Mar 2002 7:50 am Operator: Sample : gc/ms scan 3/7 Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 308:392002 iQuant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 515305 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1910027 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.20 164 1078702 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1555224 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 827010 20.00 ug/1 -0.15 44) Perylene-dl2 37.93 264 457693 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.71 235 86174 5.52 ug/mL 0.21 Spiked Amount 5.000 Recovery = 110.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.88 74 83967 4.80 ug/1 # 70 3) bis(2-Chloroethyl)ether 11.64 93 201392 7.15 ug/1 91 4) 1,3-Dichlorobenzene 12.15 146 165684 5.70 ug/1 99 5) 1,4-Dichlorobenzene 12.29 146 174441 5.98 ug/1 100 6) 1,2-Dichlorobenzene 12.81 146 173836 6.39 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.13 45 280170 7.07 ug/1 99 8) N-Nitroso-di-n-propylam'ine 13.51 70 136381 7.45 ug/1 # 86 9) Hexachloroethane 13.66 117 49396 4.53 ug/1 98 11) Nitrobenzene 13.93 77 184205 7.05 ug/1 93 12) Isophorone 14.58 82 412524 8.33 ug/1 99 13) bis(2-Chloroethoxy)methane 15.26 93 252714 7.80 ug/1 95 14) 1,2,4-Trichlorobenzene 15.77 180 154278 6.88 ug/1 97 15) Naphthalene 15.95 128 558493 7.91 ug/1 99 16) Hexachlorobutadiene 16.49 225 53974 4.83 ug/1 97 18) Hexachlorocyclopentadiene 18.68 237 15306 2.10 ug/1 95 19) 2-Chloronaphthalene 19.44 162 348863 7.53 ug/1 97 20) Dimethylphthalate 20.54 163 482882 8.90 ug/1 100 21) 2,6-Dinitrotoluene 20.75 165 97533 7.40 ug/1 # 82 22) Acenaphthylene 20.72 152 532651 8.04 ug/1 98 23) Acenaphthene 21.28 153 376903 8.14 ug/1 97 24) 2,4-Dinitrotoluene 21.92 165 122792 6.97 ug/1 # 73 25) Diethylphthalate 22.67 149 456511 8.66 ug/1 95 26) 4-Chlorophenyl-phenylether 22.82 204 208428 9.24 ug/1 90 27) Fluorene 22.80 166 420732 8.60 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 23.29 77 386773 6.85 ug/L # 82

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Tue Apr 02 13:56:26 2002 Page 1

NYC-WTC_000058835