GCMS analysis page, sample AE05034, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\5034.D Vial: 26 Acq On : 27 Mar 2002 10:31 am Operator: Sample : gc/ms scan 3/7 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Palmitic acid, 2-(trimethylsil Concentration Rank 1

R.T. EstConc Area Relative to ISTD R-.T.

0.68 ug/1 153801 Naphthalene-d8 15.89

y Hit# of 5 /Tentative ID MW MolForm CAS# Qual --------------------- y.------------------------- V 1 Palmiticz'^acid, 2 - (trimethylsiloxy) e 372 C21H44O3Si 022613-62-3 53 *^2 Cyc 1 op^tasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 49 3 Benzcy'c acid, 2,4-bis [ (trimethylsil 370 C16H30O4Si3 010586-16-0 38 4.. Benzfeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 Abundance ScanTdes^ (-) m/ z 73.00 100.00% 73

5000 267 355 —i-i-i-i'i 1111 /A 1. 11111 i-i-i-i-

45 108125 154 I77l,?3 223 2^1 14.60 14.80 15.00 15.20 ' l/'") I, I. .'l r 1;. I.... i'. . 1 .I. .7.1 fi 11 p I i+|-i Atj m/z 267.00 50.03% 40 60 80 100 120 140 160 180 200 .220 240 260 280 300 320 340 360 A *■ Abundance #51549: Palmitic acid, 2-(trimethyisiloxy)ethyIesier 7|3 116 239 5000 176 357 14.60 14.80 15.00 15.20 _ 98 313 ■m/z 355.05 49.05% I 330 S 372 A m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance =51260. Cyciepentasiloxane, decarnethyl- 73

355 ____ 14^60 14.80 15.00 15.20 267 5000 m/z'356.0,5’ 18.13%

191207 251 323339 I mfe-> ___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360_ —T-i-i-i-i-i- - ‘ ) Abundance #73975; Benzoic acid, 2,4-bis[(trTm'STyfSlyi)^^ ......... ! Th 14,60 14.80 15.00 15.20 m/z 357.0,5 12.27% 5000 355 45 I ■'33149 193 223 281 340 I 370 m/2-> 40 60 80 100 120 140 160 180 200 220 240 260 2M 300 320 340 360 14.60 14.80 15.00 15.20

5034.D GCMS0308.M Eri Mar 29 11:38:20 2002 Page 1

NYC-WTC_000058796