GCMS analysis page, sample AE01503, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR26O2\15O3.D Vial: 22 Acq On : 27 Mar 2002 6:32 am Operator: Sample : re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.84 0.41 ug/1 95450 Naphthalene-d8 15.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilo: ne, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 3,4-Dihydroxyb"-enzyl alcohol, tris (tr 356 C16H32O3Si3 068595-79-9 46 3 N-(Trifluorofecetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 43 4 Phenethylline, NlJ5®thyl2^beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 1067 (14.844 min): 1503.D (-) m/z 73 ;0^- iooToO% 73

5000 267 355 J y 45 -119 154 193 223 , 323, _ 14.60 14.80 15.00 15.20__ I I ' ' I ' ' ' I ' '''' ' I ' I ' ■' ' ' '( ' m/z 267“op' 41.10% 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 7i3

355 267 5000 I'' 14.60 14.80 15.00 15.20 m/z 355.0 40.19% I,.........207 , , , ! 323, m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49858: S.A-Dihydroxybenzy'l alcohol,insttriniethyleilyli- I 73

1A60 14.80 15.00 15.20 267 5000 179 m/ z 356.05 15.04% 356 45 147 I , 209 237 , 312 , I..................... 'm/z-> Abundance i 50

713 100 150 200 250 300 350 #60162: N-(Trifluoroacetyl)-N,O,b',d’'-tetrakis(trimethyisi 400 450 500 550 n , 14.60 14.80 15.00 15.20 m/z 267.90 11.66% 355 5000

45 ■i I 147 193 267 538 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

1503.D GCMS0308.M Fri Mar 29 11:33:41 2002 Page 1

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