Laboratory report listing analytical results for PAHs and surrogates with recovery rates on January 28, 2002.
NYC-WTC_000058153–000058154Folder label: “525 X 1/11/02 A 1/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\l\DATA\012502A\LB0111.D Vial: 13 Acq On : 25 Jan 2002 11:40 pm Operator: McLean Sample : REINJ Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:26:17 2002 Quant Results File: 012402B.RES •
Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 17.96 164 14834143 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 19630277 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 15773726 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 3825545 5.03 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.60% 19) Triphenyl Phosphate 29.33 326 3606559 6.10 ug/L 0.00 Spiked Amount 5.000 Recovery = 122.00% 21) Perylene D-12 34.02 264 10252439 4.58 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.60%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 18.71 165 5758 0.90 ug/L 21 8) Molinate 18.90 126 6626 Below Cal # 1 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 22.27 161 259624 1.28 ug/L # 1 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. 22) Bis (2-Ethylhexyl) adipate 29.32 129 61270 0.53 ug/L 67 23) Bis (2-Ethylhexyl) phthala 30.70 149 710763 0.60 ug/L 95 24) Benzo (a) pyrene 0.00 252 0 N.D. d
Q
(#) = qualifier out of range (m) = manual integration LB0111.D 012402B.M Mon Jan 28 12:27:05 2002 Page 1
NYC-WTC_000058153
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NYC-WTC_000058157
Quality control data for a calibration verification sample analysis of PAHs with recovery rates between 103 and 110 percent.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055375
Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.
1 shared topics · Same agency, volume and box · similarity 0.978
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055380
Calibration standard results for Method 525.2 listing concentrations and detection limits for target compounds.
1 shared topics · Same agency, volume and box · similarity 0.974
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058155
Instrument log showing retention times and recovery percentages for PAHs in a reference standard on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.973
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055421
Laboratory results for sample AD27986 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.970
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055481
Laboratory results for sample AD28167 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055445
Laboratory results for sample AD28047 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055439
Laboratory results for sample AD28046 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055457
Laboratory results for sample AD28104 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.967
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000057049
Laboratory report for a lab blank sample AD27232 showing non-detect results for various pesticides.
1 shared topics · Same agency, volume and box · similarity 0.967
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055385
Reference standard results for Method 525.2 verifying analytical performance for pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.967
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000082506
Results for calibration standards including deuterated compounds analyzed on May 6, 2002.
1 shared topics · similarity 0.971
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000058144
Administrative record from the Department of Environmental Protection regarding World Trade Center activities in January 2002.
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NYC-WTC_000058145
Fragmented document header containing identification codes and date ranges from the January 2002 collection.
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NYC-WTC_000058147
Lab analysis of sample AD28043 for pesticide and chemical residues, all results below method detection limits, completed Jan 29, 2002.
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NYC-WTC_000058155
Instrument log showing retention times and recovery percentages for PAHs in a reference standard on January 28, 2002.
Filed in the same folder
NYC-WTC_000058157
Quality control data for a calibration verification sample analysis of PAHs with recovery rates between 103 and 110 percent.
Filed in the same folder