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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10130 Sample Date/Time: Tuesday, May 14, 2002 13:17:16 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd 1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE1 0130.054 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 11.667 17.843 0.000 0.00900 55.24 ug/L Sc-1 45 529314.603 0.711 529314.603 ug/L Cr 52 9594.156 0.550 0.003 0.14341 7.47 ug/L Cr 53 2304.315 2.806 0.003 1.14651 3.94 ug/L Mn 55 383524.350 0.314 0.723 20.13498 1.03 ug/L Ni 60 937.391 4.139 0.002 0.32248 5.03 ug/L Cu 63 6494.385 2.869 0.012 1.03706 3.57 ug/L Cu 65 3091.223 3.108 0.006 1.02844 2.83 ug/L Zn 66 9161.706 1.026 0.070 4.14569 1.99 ug/L Zn 67 1695.508 2.487 0.013 4.35902 3.36 ug/L Zn 68 7413.096 1.378 0.057 4.52518 1.09 ug/L > Ge 72 117075.329 1.584 117075.329 ug/L As 75 6319.973 2.014 0.009 0.45909 19.75 ug/L Se 77 887.392 3.550 0.001 0.54830 37.20 ug/L Se 82 -33.473 99.461 -0.000 -0.07647 162.09 ug/L Kr 83 2162.279 1.411 -342.425 ug/L Ag 107 94.335 10.405 -0.000 -0.01600 4.54 ug/L in 115 1544841.404 0.844 1544841.404 ug/L Sb 121 502.686 6.659 0.000 0.04957 6.36 ug/L Sb 123 387.735 7.363 0.000 0.04955 8.59 ug/L Ba 135 53070.328 1.060 0.020 15.56994 0.50 ug/L Ba 137 93673.759 0.831 0.035 15.62687 0.68 ug/L > Tb 159 2647622.636 0.762 2647622.636 ug/L Hg 201 46.667 7.525 0.000 0.00063 342.58 ug/L Hg 202 88.335 20.007 -0.000 -0.00164 289.74 ug/L TI 205 916.722 2.968 -0.000 -0.00066 91.27 ug/L Pb 208 5403.020 0.871 0.001 0.05080 3.20 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 75.112 Cr 52 Cr 53 Mn 55

Sample ID: AE10130 Report Date/Time: Tuesday, May 14, 2002 13:18:57 Page 1

NYC-WTC_000053496

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