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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09449 Sample Date/Time: Wednesday, May 08, 2002 13:29:46 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09449.810 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 16.334 49.487 0.000 0.01776 134.54 ug/L Sc-1 45 444520.359 2.271 444520.359 ug/L Cr 52 7852.136 1.895 0.002 0.07929 15.04 ug/L Cr 53 1814.866 3.400 0.002 0.91783 9.00 ug/L Mn 55 362115.348 2.825 0.801 21.81682 2.96 ug/L Ni 60 1207.426 4.285 0.003 0.42975 6.12 ug/L Cu 63 111859.818 1.093 0.251 19.12559 3.06 ug/L Cu 65 54994.746 1.444 0.123 19.13414 3.56 ug/L Zn 66 4561.857 0.716 0.033 2.00506 2.82 ug/L Zn 67 938.725 3.099 0.007 2.24025 3.37 ug/L Zn 68 3986.581 2.373 0.029 2.32172 1.92 ug/L Ge 72 116438.922 1.769 116438.922 ug/L As 75 11353.776 0.243 0.008 0.36838 21.61 ug/L Se 77 1436.955 0.807 0.000 0.24221 28.04 ug/L Se 82 -130.418 61.207 -0.001 -0.27935 110.91 ug/L Kr 83 4067.951 2.050 -393.522 ug/L Ag 107 172.337 2.197 -0.000 -0.01435 1.86 ug/L > In 115 1709919.299 0.070 1709919.299 ug/L Sb 121 681.699 4.355 0.000 0.04869 5.16 ug/L Sb 123 519.943 7.832 0.000 0.04742 9.67 ug/L Ba 135 59158.452 0.421 0.023 15.83604 0.88 ug/L Ba 137 103648.235 0.789 0.041 15.84464 1.33 ug/L > Tb 159 2544179.905 1.084 2544179.905 ug/L Hg 201 103.668 5.485 -0.000 -0.00833 46.66 ug/L Hg 202 216.005 6.914 -0.000 -0.00936 46.62 ug/L TI 205 844.715 8.442 -0.000 -0.01809 8.89 ug/L Pb 208 18034.887 1.585 0.006 0.29466 2.03 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ’ Be 9 > Sc-1 45 86.929 Cr 52 Cr 53 Mn 55

Sample ID: AE09449 Report Date/Time: Wednesday, May 08, 2002 13:31:26 Page 1

NYC-WTC_000053163

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