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ICPMS daily performance check report, May 3, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 3, 2002.

NYC-WTC_000052963–000053092

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08955 Sample Date/Time: Friday, May 03,2002 14:46:56 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\_NEWN.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE08955.743 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 7.333 56.773 -0.000 -0.00534 158.04 ug/L > Se-1 45 506864.087 0.557 506864.087 ug/L Cr 52 8277.851 2.492 0.001 0.02833 84.10 ug/L Cr 53 2454.023 5.535 0.003 1.41107 7.18 ug/L Mn 55 592029.112 2.542 1.164 34.79983 3.01 ug/L Ni 60 2428.349 3.075 0.004 0.92970 3.69 ug/L Cu 63 7753.383 2.100 0.015 1.46855 2.74 ug/L Cu 65 3089.889 1.910 0.006 1.14804 2.60 ug/L Zn 66 2280.309 2.463 0.012 0.68117 9.02 ug/L Zn 67 658.364 3.599 0.004 1.35971 8.00 ug/L Zn 68 2557.385 1.275 0.017 1.33173 4.27 ug/L Ge 72 99641.950 2.362 99641.950 ug/L As 75 8208.035 1.312 0.006 0.29081 52.06 ug/L Se 77 1186.485 0.270 0.002 0.97878 16.29 ug/L Se 82 2930.168 0.242 0.000 0.20027 178.84 ug/L Ag 107 899.387 14.491 0.001 0.06520 17.45 ug/L Cd 111 56.667 20.301 0.000 0.00214 193.74 ug/L Cd 114 132.186 25.304 0.000 0.00210 257.54 ug/L > in 115 1152097.810 2.902 1152097.810 ug/L Sb 121 937.058 9.036 0.001 0.11671 6.83 ug/L Sb 123 723.722 6.765 0.001 0.11750 4.52 ug/L Ba 135 68380.052 3.110 0.039 27.09359 0.83 ug/L Ba 137 126011.252 0.393 0.072 29.54136 2.96 ug/L Ho 165 1709702.232 0.468 0.030 ug/L > Tb 159 1742743.761 2.650 1742743.761 ug/L Hg 201 83.335 12.490 0.000 0.02030 36.33 ug/L Hg 202 165.003 3.149 0.000 0.02294 3.87 ug/L TI 205 551.022 8.915 -0.000 -0.00344 42.22 ug/L Pb 208 3668.326 3.927 0.001 0.05112 2.87 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 82.699 Cr 52

Sample ID: AE08955 Report Date/Time: Friday, May 03, 2002 14:48:43 Page 1

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