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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09517 Sample Date/Time: Wednesday, May 08, 2002 14:36:59 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09517.819 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 13.333 37.749 0.000 0.00944 151.60 ug/L > Se-1 45 439460.613 0.366 439460.613 ug/L Cr 52 7689.330 3.708 0.002 0.07156 40.66 ug/L Cr 53 1468.133 2.561 0.002 0.63491 4.83 ug/L Mn 55 298893.760 0.439 0.666 18.14990 0.15 ug/L Ni 60 863.050 0.505 0.002 0.30121 0.92 ug/L Cu 63 6441.013 1.922 0.014 1.07720 1.62 ug/L Cu 65 3164.583 2.877 0.007 1.06076 3.27 ug/L Zn 66 1525.477 1.217 0.007 0.44987 0.99 ug/L Zn 67 457.016 7.479 0.003 0.88831 12.78 ug/L Zn 68 1742.518 2.046 0.010 0.81766 3.07 ug/L > Ge 72 114049.798 1.068 114049.798 ug/L As 75 10609.674 1.087 0.003 0.15106 14.30 ug/L Se 77 1340.125 1.440 -0.000 -0.07269 92.79 ug/L Se 82 -104.931 41.150 -0.000 -0.18920 88.22 ug/L Kr 83 3745.142 0.931 -716.330 ug/L Ag 107 362.344 4.862 -0.000 -0.00081 176.81 ug/L > In 115 1675585.496 2.221 1675585.496 ug/L Sb 121 767.040 1.754 0.000 0.05734 2.11 ug/L Sb 123 600.796 3.800 0.000 0.05783 2.83 ug/L Ba 135 55382.463 2.317 0.022 14.70769 0.55 ug/L Ba 137 96407.390 2.834 0.038 14.62037 1.58 ug/L > Tb 159 2564022.661 1.764 2564022.661 ug/L Hg 201 122.002 7.146 0.000 0.00162 272.94 ug/L Hg 202 264.006 9.797 0.000 0.00228 258.13 ug/L TI 205 906.721 10.881 -0.000 -0.01669 12.89 ug/L Pb 208 4633.842 1.904 0.001 0.03499 1.80 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 85.939 Cr 52 Cr 53 Mn 55

Sample ID: AE09517 Report Date/Time: Wednesday, May 08, 2002 14:38:40 Page 1

NYC-WTC_000053181

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