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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09450 Sample Date/Time: Wednesday, May 08, 2002 13:34:46 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE09450.811 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 16.667 18.330 0.000 - 0.01849 45.23 ug/L > Se-1 45 443770.834 0.642 443770.834 ug/L Cr 52 8042.638 2.237 0.002 0.10007 14.26 ug/L Cr 53 1650.500 1.091 0.002 0.77867 1.46 ug/L Mn 55 314898.837 1.446 0.696 18.95178 0.97 ug/L Ni 60 1253.766 2.096 0.003 0.44806 2.72 ug/L Cu 63 58732.379 1.122 0.132 10.03694 1.72 ug/L Cu 65 29086.099 2.543 0.065 10.10677 3.17 ug/L Zn 66 4813.989 0.928 0.036 2.13937 1.26 ug/L Zn 67 990.397 2.303 0.007 2.39355 3.41 ug/L Zn 68 4161.661 3.167 0.031 2.44654 4.46 ug/L > Ge 72 116231.837 0.756 116231.837 ug/L As 75 11491.553 2.081 0.009 0.43361 29.50 ug/L Se 77 1442.813 1.429 0.001 0.28054 48.02 ug/L Se 82 -65.353 250.858 -0.000 -0.02947 2117.81 ug/L Kr 83 4025.598 1.948 -435.874 ug/L Ag 107 191.337 6.103 -0.000 -0.01299 7.73 ug/L > in 115 1703821.053 1.492 1703821.053 ug/L Sb 121 625.028 3.910 0.000 0.04403 3.52 ug/L Sb 123 480.861 3.757 0.000 0.04327 6.46 ug/L Ba 135 55585.649 0.895 0.022 14.97454 1.22 ug/L Ba 137 97150.984 0.285 0.038 14.94555 0.32 ug/L > Tb 159 2527855.610 0.497 2527855.610 ug/L Hg 201 83.668 9.952 -0.000 -0.01955 24.78 ug/L Hg 202 189.337 1.698 -0.000 -0.01587 5.59 ug/L TI 205 787.042 6.405 -0.000 -0.01943 6.76 ug/L Pb 208 18832.473 1.716 0.006 0.31239 1.53 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff Be 9 > Sc-1 45 86.782 Cr 52 Cr 53 Mn 55

Sample ID: AE09450 Report Date/Time: Wednesday, May 08, 2002 13:36:27 Page 1

NYC-WTC_000053165

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