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ICPMS daily performance check report, May 8, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 8, 2002.

NYC-WTC_000053094–000053210

Folder label: “ICPMS 5/3/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE09575 Sample Date/Time: Wednesday, May 08, 2002 15:14:47 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\new york cit\AE09575.830 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 12.667 9.116 0.000 - 0.00716 43.43 ug/L > Se-1 45 444094.948 0.424 444094.948 ug/L Cr 52 11399.257 0.733 0.010 0.44414 2.25 ug/L Cr .53 2148.275 3.339 0.003 1.20317 4.44 ug/L Mn 55 259871.304 2.454 0.571 15.56258 2.09 ug/L Ni 60 859.716 3.374 0.002 0.29640 3.31 ug/L Cu 63 5694.173 1.852 0.012 0.93756 1.65 ug/L Cu 65 2798.792 1.588 0.006 0.92132 1.23 ug/L Zn 66 2989.188 2.824 0.020 1.21525 2.61 ug/L Zn 67 687.366 3.419 0.005 1.55212 5.75 ug/L Zn 68 2762.114 2.539 0.019 1.51785 4.12 ug/L > Ge 72 114607.416 1.044 114607.416 ug/L As 75 10578.197 1.171 0.002 0.11592 21.63 ug/L Se 77 1366.573 2.817 0,000 0.01981 884.53 ug/L Se 82 8.675 663.658 0.001 0.25058 88.96 ug/L Kr 83 3642.433 0.199 -819.040 ug/L Ag 107 141.669 15.487 -0.000 -0.01613 9.19 ug/L In 115 1653820.544 0.993 1653820.544 ug/L Sb 121 592.025 4.100 0.000 0.04275 5.32 ug/L Sb 123 465.479 3.673 0.000 0.04308 3.33 ug/L Ba 135 52945.270 1.177 0.021 14.01436 1.11 ug/L Ba 137 92801.521 0.316 0.036 14.02781 0.32 ug/L > Tb 159 2572490.762 0.214 2572490.762 ug/L Hg 201 84.001 5.189 -0.000 -0.02021 11.78 ug/L Hg 202 158.003 1.096 -0.000 -0.02460 2.01 ug/L TI 205 683.699 9.314 -0.000 -0.02241 7.11 ug/L Pb 208 4564.831 2.300 0.001 0.03338 5.57 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 > Sc-1 45 86.846 Cr 52 Cr 53 Mn 55

Sample ID: AE09575 Report Date/Time: Wednesday, May 08, 2002 15:16:27 Page 1

NYC-WTC_000053201

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