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ICPMS daily performance check report, May 14, 2002

Machine-extracted title · confidence 98%

Daily instrument calibration and performance verification log for ICPMS equipment conducted on May 14, 2002.

NYC-WTC_000053389–000053503

Folder label: “ICPMS 5/14/02”

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE10065 Sample Date/Time: Tuesday, May 14, 2002 13:08:11 Sample Type: Sample Sample Description: Number of Replicates: 3 Method File: c:\winnt\profiles\lrd1\elandata\Method\NEWQ200.8.mth Dataset File: c:\winnt\profiles\lrd1\elandata\Dataset\newyork cit\AE1 0065.051 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Conc. Mean Cone. RSD Sample Unit Be 9 10.000 26.458 0.000 0.00550 108.69 ug/L Se-1 45 520717.446 0.971 520717.446 ug/L Cr 52 8669.554 2.523 0.002 0.07442 33.81 ug/L Cr 53 2071.924 3.140 0.003 0.99939 6.43 ug/L Mn 55 376490.350 1.021 0.721 20.09146 0.94 ug/L Ni 60 1149.084 3.805 0.002 0.40462 3.38 ug/L Cu 63 52145.655 0.935 0.100 8.81143 1.36 ug/L Cu 65 24991.222 1.024 0.048 8.82103 1.68 ug/L Zn 66 5200.539 0.283 0.037 2.19280 2.13 ug/L Zn 67 1087.076 6.327 0.008 2.66486 8.85 ug/L Zn 68 4482.817 2.663 0.033 2.59552 3.85 ug/L Ge 72 115254.919 1.485 115254.919 ug/L As 75 6546.603 2.960 0.012 0.59527 7.04 ug/L Se 77 892.511 0.896 0.001 0.63266 4.06 ug/L Se 82 36.996 168.380 0.000 0.18888 126.30 ug/L Kr 83 2148.609 0.310 -356.095 ug/L Ag 107 147.336 4.519 -0.000 -0.01194 3.01 ug/L > In 115 1534338.323 1.516 1534338.323 ug/L Sb 121 586.025 2.649 0.000 0.05873 2.13 ug/L Sb 123 430.615 1.938 0.000 0.05584 0.46 ug/L Ba 135 52539.584 0.936 0.020 15.69245 1.18 ug/L Ba 137 90364.818 0.832 0.035 15.34624 1.10 ug/L Tb 159 2600777.823 0.272 2600777.823 ug/L Hg 201 60.334 10.656 0.000 0.00957 40.99 ug/L Hg 202 115.335 6.508 0,000 0.00607 34.42 ug/L TI 205 881.718 7.242 -0.000 -0.00114 148.68 ug/L Pb 208 17280.623 0.719 0.006 0.29755 1.03 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rel. % Diff Be 9 Se-1 45 73.892 Cr 52 Cr 53 Mn 55

Sample ID: AE10065 Report Date/Time: Tuesday, May 14, 2002 13:09:52 Page 1

NYC-WTC_000053490

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