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GCMS analysis results for sample AE01404, Feb 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01404 conducted on February 27, 2002.

NYC-WTC_000052953–000052961

Folder label: “GCMS X 1/10/02 A 2/19/02

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op' 404 P 10 £91902 Mu JDMP pr Quantitation Report (QT Reviewed)

C:\HPCHEM\l\DATA\FEB1902\14 04.D Vial: 13 : 19 Feb 2002 10:03 pm Operator: 209 Data : gc/ms scan 1/18 Inst : GC/N Acq Multiplr: 1.00 Sam Migration Params: GOOFY. P Me Time: Feb 21 15:02 2002 Quant Results File: GCMSC O ant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) itle : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min

1) 1,4-Dichlorobenzene-d4 12.33 152 300413 20.00 ug/1 -0.01 10) Naphthalene-d8 15.98 136 1134914 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.29 164 578426 20.00 ug/1 -0.02 29) Phenanthrene-diO 25.73 188 814179 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 513890 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 349847 20.00 ug/1 -0.04

System Monitoring Compounds 37) 2,4-DDD 30.81 235 37113 4.54 ug/mL 0.31 Spiked Amount 5,000 Recovery = 90.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 4 ,4 -Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2* oxybis (1-Chloropropan 0.00 45 0 N.D. 8) N-Nitoso-di-n-propylamine 0.00 70 0 N.D. 9) Hexacoroethane 0.00 117 0 N.D. 11) NitlOnzene 0.00 77 0 N.D. 12) IsoPhne 0.00 82 0 N.D. 13) bis (2 oroethoxy) methane 0.00 93 0 N.D. 14) 112•4 chlorobenzene 0.00 180 0 N.D. 15) Naphthe 16.03 128 699 N.D. 16) Hexacutadiene 0.00 225 0 N.D. 18) Hexach yclopentadiene 0.00 237 0 N.D. 19) 2-chlor thalene 0.00 162 20 pimethylalate 0.00 163 0 N.D. 21 2,6-Dilluene 25 AcenaphtE 0.00 165 0 0 N.D. N.D. rat 0.00 152 0 N.D. 02 0.00 153 22)29) BipGokOrC eenyiphesnehenylether 0.00 165 22.75 149 0.00 204 235 0 0 0 N.D. N.D. N.D. N.D. 0.00 166 0 N.D. 2 8) ______________ pheny ihyd 0.00 77 0 N.D. - -ifier C - — - - (#) = GA80208 ange (m) = manual integration 1404.D CC Thu Feb 21 15:07:33 2002

NYC-WTC_000052955

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NYC-WTC_000052955Source: NYC Law Department, mirrored locally

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