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Quantitation Report (QT Reviewed)
C:\HPCHEM\l\DATA\FEB1902\14 04.D Vial: 13
: 19 Feb 2002 10:03 pm Operator: 209
Data : gc/ms scan 1/18 Inst : GC/N
Acq Multiplr: 1.00
Sam
Migration Params: GOOFY. P
Me Time: Feb 21 15:02 2002 Quant Results File: GCMSC
O
ant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
itle : 209 625/TCLP calibration table
Last Update : Wed Feb 13 11:43:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min
1) 1,4-Dichlorobenzene-d4 12.33 152 300413 20.00 ug/1 -0.01
10) Naphthalene-d8 15.98 136 1134914 20.00 ug/1 -0.02
17) Acenaphthene-diO 21.29 164 578426 20.00 ug/1 -0.02
29) Phenanthrene-diO 25.73 188 814179 20.00 ug/1 -0.03
38) Chrysene-dl2 33.80 240 513890 20.00 ug/1 -0.04
44) Perylene-dl2 38.08 264 349847 20.00 ug/1 -0.04
System Monitoring Compounds
37) 2,4-DDD 30.81 235 37113 4.54 ug/mL 0.31
Spiked Amount 5,000 Recovery = 90.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 4 ,4 -Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2* oxybis (1-Chloropropan 0.00 45 0 N.D.
8) N-Nitoso-di-n-propylamine 0.00 70 0 N.D.
9) Hexacoroethane 0.00 117 0 N.D.
11) NitlOnzene 0.00 77 0 N.D.
12) IsoPhne 0.00 82 0 N.D.
13) bis (2 oroethoxy) methane 0.00 93 0 N.D.
14) 112•4 chlorobenzene 0.00 180 0 N.D.
15) Naphthe 16.03 128 699 N.D.
16) Hexacutadiene 0.00 225 0 N.D.
18) Hexach yclopentadiene 0.00 237 0 N.D.
19) 2-chlor thalene 0.00 162
20 pimethylalate 0.00 163
0 N.D.
21 2,6-Dilluene
25 AcenaphtE 0.00 165
0
0
N.D.
N.D. rat
0.00 152 0 N.D. 02
0.00 153
22)29) BipGokOrC
eenyiphesnehenylether 0.00 165
22.75 149
0.00 204
235
0
0
0
N.D.
N.D.
N.D.
N.D.
0.00 166 0 N.D.
2 8) ______________ pheny ihyd 0.00 77 0 N.D.
- -ifier C - — - -
(#) = GA80208 ange (m) = manual integration
1404.D CC Thu Feb 21 15:07:33 2002
NYC-WTC_000052955
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