NYC-WTC_000006302
Initial GCMS analysis report for sample AE03389 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
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GCMS Sample AE03388 Report, March 12 2002
Machine-extracted title · confidence 95%Initial GCMS analysis report for sample AE03388 conducted by analyst DLV on March 12, 2002.
NYC-WTC_000006292–000006301Folder label: “GCMS X 2/14/02 A 2/23/02”
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NYe9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB2102\3388.D Vial: 50 Acq On : 23 Feb 2002 5:22 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 8 9:23 2002 <Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.33 152 233674 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 890819 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.28 164 472875 20.00 ug/1 -0.03 29) Phenanthrene-diO 25.74 188 656092 20.00 ug/1 -0.03 38) Chrysene-dl2 33.81 240 432126 20.00 ug/1 -0.04 44) Perylene-dl2 38.08 264 294091 20.00 ug/1 -0.04
System Monitoring Compounds 37) 2,4-DDD 30.81 235 45329 K 303 6.62 ug/mL 0.32 Spiked Amount 5.000 Recovery = 132.10%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. .6) Hexachlorobutadiene 0.00 225 0 N.D. 8) Hexachlorocyclopentadiene 0.00 237 0 N.D. 9) 2-Chloronaphthalene 0.00 162 0 N.D. 0) Dimethylphthalate 0.00 163 0 N.D. 1) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2) Acenaphthylene 0.00 152 0 N.D. ) Acenaphthene 0.00 153 0 N.D. ) 2,4-Dinitrotoluene 0.00 165 0 N.D. ) Diethylphthalate 0.00 149 0 N.D. ) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. ) Fluorene 0.00 166 0 N.D. Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
= qualifier out of range (m) = manual integration .D GCMS0208.M Fri Mar 08 09:24:26 2002 Page 1
NYC-WTC_000006294
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