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GCMS analysis results for sample AE01336, Feb 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of sample AE01336 conducted on February 27, 2002.

NYC-WTC_000052909–000052917

Folder label: “GCMS X 1/10/02 A 2/19/02

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NYc 9r11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\FEB1902\1336.D Vial: 10 Acq On : 19 Feb 2002 7:09 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 21 14:38 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 285578 20.00 ug/1 -0.02 10) Naphthalene-d8 15.98 136 1084198 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.28 164 549733 20.00 ug/1 -0.03 29) Phenanthrene-diO 25.74 188 770503 20.00 ug/1 -0.03 38) Chrysene-dl2 33.80 240 489260 20.00 ug/1 -0.05 44) Perylene-dl2 38.07 264 322213 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 30.81 235 39742 5.14 ug/mL 0.31 Spiked Amount 5.000 Recovery = 102.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2‘-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. .3) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 4) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 5) Naphthalene 16.03 128 740 N.D. 6) Hexachlorobutadiene 0.00 225 0 N.D. 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. )) 2-Chloronaphthalene 0.00 162 0 N.D. 1) Dimethylphthalate 0.00 163 0 N.D. ) 2,6-Dinitrotoluene 0.00 165 0 N.D. ) Acenaphthylene 0.00 152 0 N.D. ) Acenaphthene 0.00 153 0 N.D. 2,4-Dinitrotoluene 0.00 165 0 N.D. Diethylphthalate 0.00 149 0 N.D. 4-Chlorophenyl-phenylether 0.00 204 0 N.D. Fluorene 0.00 166 0 N.D. Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

= qualifier out of range (m) = manual integration D GCMS0208.M Thu Feb 21 14:39:04 2002 Page 1

NYC-WTC_000052911

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NYC-WTC_000052911Source: NYC Law Department, mirrored locally

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