GCMS analysis report for sample AE01231, Feb 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\FEB1802\1231.D Vial: 38 Acq On : 18 Feb 2002 2:10 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 20 15:35 2002 <Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 13 11:43:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.33 152 227569 20.00 ug/1 -0.02 10) Naphthalene-d8 15.97 136 849721 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.28 164 445114 20.00 ug/1 -0.03 29) Phenanthrene-diO 25.73 188 587763 20.00 ug/1 -0.03 38) Chrysene-dl2 33.79 240 363234 20.00 ug/1 -0.05 44) Perylene-dl2 38.07 264 239940 20.00 ug/1 -0.05

System Monitoring Compounds 37) 2,4-DDD 30.81 235 31972 5.42 ug/mL 0.31 Spiked Amount 5.000 Recovery = 108.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.73 93 287 N.D. 4) 1,3-Dichlorobenzene 12.38 146 310 N.D. 5) 1,4-Dichlorobenzene 12.38 146 310 N.D. 6) 1,2-Dichlorobenzene 12.90 146 289 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 14.02 77 215 N.D. 12) Isophorone 14.68 82 841 N.D. 13) bis(2-Chloroethoxy)methane 15.34 93 315 N.D. 14) 1,2,4-Trichlorobenzene 15.85 180 191 N.D. 15) Naphthalene 16.02 128 1906 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.54 162 505 N.D. 20) Dimethylphthalate 20.63 163 565 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.82 152 692 N.D. 2 3) Acenaphthene 21.37 153 646 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.76 149 945 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.90 166 631 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1231.D GCMS0208.M Wed Feb 20 15:36:30 2002 Page 1

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