NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB0802\30707.D Vial: 50
Acq On : 10 Feb 2002 10:48 am Operator: 209 GALOS
Sample : GC/MS SCAN 2/8 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 14 16:27 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Wed Feb 13 11:43:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.35 152 424040 20.00 ug/1 0.00
10) Naphthalene-d8 15.99 136 1644143 20.00 ug/1 0.00
17) Acenaphthene-diO 21.31 164 877118 20.00 ug/1 0.00
29) Phenanthrene-diO 25.76 188 1288841 20.00 ug/1 0.00
38) Chrysene-dl2 33.82 240 896694 20.00 ug/1 -0.02
44) Perylene-dl2 38.11 264 594668 20.00 ug/1 -0.02
System Monitoring Compounds
37) 2,4-DDD 30.83 235 51528 3.98 ug/mL 0.33
Spiked Amount 5.000 Recovery = 79.60%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.99 74 525 N.D.
3) bis(2-Chloroethyl)ether 11.74 93 1068 N.D.
4) 1,3-Dichlorobenzene 12.25 146 1348 N.D.
5) 1,4-Dichlorobenzene 12.39 146 1692 N.D.
6) 1,2-Dichlorobenzene 12.91 146 1326 N.D.
7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.76 117 261 N.D.
11) Nitrobenzene 14.04 77 970 N.D.
12) Isophorone 14.69 82 1841 N.D.
13) bis(2-Chloroethoxy)methane 15.35 93 1325 N.D.
14) 1,2,4-Trichlorobenzene 15.87 180 1182 N.D.
15) Naphthalene 16.05 128 4569 N.D.
16) Hexachlorobutadiene 16.59 225 621 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 19.55 162 2334 N.D.
20) Dimethylphthalate 20.64 163 2549 N.D.
21) 2,6-Dinitrotoluene 20.85 165 110 N.D.
22) Acenaphthylene 20.83 152 2527 N.D.
2 3) Acenaphthene 21.39 153 2610 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.78 149 2761 N.D.
26) 4-Chlorophenyl-phenylether 22.94 204 1282 N.D.
27) Fluorene 22.91 166 2542 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30707. D GCMS0208.M Thu Feb 14 16:28:29 2002 Page 1
NYC-WTC_000004432
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