GCMS reference results for sample AE05845, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR2302\REFA2.D Vial: 18 Acq On 24 Apr 2002 6:57 am Operator : Sample gc/ms scan 4/17 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 11:16 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 486741 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1788924 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1016155 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1501384 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 960015 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 590163 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 23.29 209 45616 8.96 ug/L -0.04 Spiked Amount 10.000 Recovery = 89.60% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 99244 9.37 ug/1 95 3) bis(2-Chloroethyl)ether 11.60 93 251231 15.24 ug/1 98 4) 1,3-Dichlorobenzene 12.11 146 191030 11.23 ug/1 100 5) 1,4-Dichlorobenzene 12.25 146 198922 11.63 ug/1 98 6) 1,2-Dichlorobenzene 12.77 146 197456 12.43 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.09 45 348375 15.29 ug/1 99 8) N-Nitroso-di-n-propylamine 13.48 70 159928 14.79 ug/1 99 9) Hexachloroethane 13.62 117 56668 9.04 ug/1 92 11) Nitrobenzene 13.89 77 227623 14.51 ug/1 100 12) Isophorone 14.54 82 364571 12.28 ug/1 97 13) bis(2-Chloroethoxy)methane 15.22 93 299483 15.49 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 177265 13.03 ug/1 98 15) Naphthalene 15.90 128 641171 14.91 ug/1 100 16) Hexachlorobutadiene 16.44 225 63632 9.36 ug/1 99 18) Hexachlorocyclopentadiene 18.63 237 6272 1.40 ug/1 97 19) 2-Chloronaphthalene 19.41 162 397693 14.84 ug/1 98 20) Dimethylphthalate 20.49 163 521620 16.88 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 107868 14.60 ug/1 97 22) Acenaphthylene 20.67 152 586660 15.65 ug/1 100 23) Acenaphthene 21.24 153 423305 15.88 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 137867 14.18 ug/1 96 25) Diethylphthalate 22.63 149 497971 16.80 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 223098 16.97 ug/1 96 27) Fluorene 22.76 166 475362 16.84 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 436459 13.92 ug/L 98 31) N-Nitrosodiphenylamine 23.17 168 143059 11.45 ug/1 97 32) 4-Bromophenyl-phenylether 24.24 248 125070 17.16 ug/1 97

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Wed Apr 24 11:18:22 2002 Page 1

NYC-WTC_000046474