GCMS analysis results for sample AE01332, Feb 2002

NYC 9/11 Public Portal Document

LLOLCLY DCa-tia UWp

Data File : C:\HPCHEM\1\DATA\FEB1902\1332.D Vial: 5 Acq On : 19 Feb 2002 2:07 pm Operator: 209 GALOS Sample : gc/ms scan 1/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.29 ug/1 21843 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 /) Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane 74 C3H602 000646-06-0 7 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 Formamide, N, N-dimethyl - 73 C3H7NO 000068-12-2 4 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 3 Abundance Scan 345 (8.208 min): 1332.D (-) m/z73.00100.00% 73

5000 43 /

। — । i m । i i i > । i i i > । i i i i । > i 11 n mill + 51 69, P 11 ■ m/z 43.05 8.4028.97% 7.80 8.00 _ 8.60 8.20 Th I' " ' I > i ■■■ • 11 > • ■ । ‘11 m/z- 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4! r ' rr #62557: 1,3-Dioxolane 73

5000 29 44 7.80 8.00 8.20 NJ 8.40 8.60 5 m/ z 40.9.5 11.09%

m/z-> 19 26 TTTTTTTTTTTTTTT m 111 r1^11 r l " " I " " I T’TTTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 v Abundance 30 73 ’ 7.80 8.00 8.20 8.40 8.60 5000 m/z 45.05 10.36% 44 58 27 15 41 r ■'' i'''1 i'''' i ’ " ' i1 ' i ■ ■'' i r ' " i1''' i' ■ ■ ■ i" ' ‘ r ''' i' ■'' i ’'1' i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62527: Formamide, N,N-dimethyl- 1 ' H ' 1 ' | I ! 44 73 j 7.80 8.00 8.20 8.40__ 8.60 ’ m/z 71.10 6.54% 5000- 30 15

miz- i " " r ■ +3L 27 1 ■ < |1 ■ ■11 ■ I •11 ■ 1T 58 I ‘" i ’1" i11'' i" " i " '11' 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1332.D GCMS0208.M Thu Feb 21 15:26:02 2002 Page 1

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