GCMS Sample AE03436 Report, March 12 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\FEB2102\3436.D Vial: 56 Acq On : 23 Feb 2002 11:16 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 3.92 ug/1 277337 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 j Tentative ID MW MolForm CAS# Qual ___________ 1 1 1,3-Dioxplane, 2-methyl- 88 C4H802 000497-26-7 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 ICQ . 00% 9 Abundance ' Scan 344 (8.198 min): 3436.D (-) 1 m] 73.00 78 ■

5000 43 ,1 . ... ; , 87 103 7.80 8.00 8.20 8.40 8.60 ....................... 111 50 55., . 67 । ■ ' । ■ ■ i 1 1 ■ 1 1 1 1 1 ' I 1 ' ■ ' i ■ > ■ । I-'-1'"' -1 l 1 I > > I ■ ■ 111 t ■ > ■ 1 I 111 ‘ ' I 1 m/z 42.95 29.83% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902; 1.3-Dioxolane, 2-methyl- 73

5000 43 7.80 8.00 8.20 8.40_ 8.60j 58 m/z 41.05 10.93% 27 | 1 ' lr 1 1 1 1 1 1 1,1 l!| 1 1 1 1 1 1 ' 1 I ‘ ' 1 I ' ' ' ' I ' 1 ' ' I ' ' ' ' I ' ' 1 ' I ' ' 1 ' I ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 30

7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 10.14%

15 41 55 70 87 ' ' i ' ' ' ' i 1 ' ' ' i ' 1 ' 1 i ' ' ' ' i ' ' 1 ' i ' 1 1 1 1 1 ' 1 1 I 1 1 1 1 I ' 1 1 1 1 1 1 1 1 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 3b #292: N-Ethylformamide 7.80 1 Im । । । । । । । 8.00 8.20 8.40_ 8.60 73 m/ z 71.00 7.14% 5000 44 58

15 ' ' [ 1 1 ' ' I * < I ' -- ' | ■ 1 ■ | r ‘ | । | t -J ' i । i i > ■ । i m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

3436.D GCMS0208.M Fri Mar 08 09:49:41 2002 Page 1

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