GCMS Sample AE03436 Report, March 12 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\FEB2102\3436.D Vial: 56 Acq On : 23 Feb 2002 11:16 pm Operator: Sample : gc/ms scan 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.29 0.78 ug/1 55512 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4 - hydroxy - 4 pethy1 - 116 C6H1202 000123-42-2 36 2 5-Hexen-2-one 98 C6H10O 000109-49-9 9 3 1,8-Nonanediol , 8-methyl- 174 C10H22O2 054725-73-4 9 4 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 100.00% 5 Abundance Scan 354 (8.290 min): 3436.D (-) m/ z 43 59 5000 101 / 11t/d///d/0/m 8.00 8.20 _ 8.40 8.60 __ m/z-> 10 20 PPP4+ 30 40 •49—+ 60 6970 50 83 i ■ ■ ■ ■ i ■ 1 ■ ' i ■ 1 ' 1 i ' 1 1 1 i ■ ■ ■ 1 i ' 1 1 1 1 1 1 1 ' 1 1 80 90 100 110 120 130 m/ z 59.05 54.80% Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000- 59 .... /V...... ____ 8.00 8.20 8.40 8.60_____ m/z 100.95 23.23% 15 31 101 83 1 ' i ■ 1 1 ' i 1 ' 1 ' i 1 1 1 1 i ' 1 1 ‘ i 1 ' ' 1 i ' ' ' ' i r 1 ■ ' i ' 1 i 1 1 1 1 I 1 1 ' 1 1 ' ' 1 1 1 1 1 1 ' 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 43

___ 8.00 8.20 8.40 8.60 i 5000 m/ z 58.05 22.75%

27 55 15 83 98 '1111 r ■ । ■ ■ ■ ■ ।1' ■ ‘ ।1 ■ ■11r 1 ■ ■ । ■ ■ ■ ■ ।1111111 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ' ■ । l i > > । I ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16264: 1,8-Nonanediol, 8-methyl- 59 8.00 8.20 8.40 8.60 m/ z 41,. 05 7.56% 5000-

42 69 83 98 123 m/z-> —IPOPIPTPPIT h ' 11’1 ' ' ' i ■ ■ ■ • । । । ■ 1 10 20 30 40 50 (60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

3436.D GCMS0208.M Fri Mar 08 09:49:46 2002 Page 2

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